More than three decades ago, at Fraunhofer IZFP, research activities that were related to the application of micromagnetic methods for nondestructive testing (NDT) of the microstructure and the properties of ferrous materials commenced. Soon, it was observed that it is beneficial to combine the measuring information from several micromagnetic methods and measuring parameters. This was the birth of 3MA—the micromagnetic multi-parametric microstructure and stress analysis. Since then, 3MA has undergone a remarkable development. It has proven to be one of the most valuable testing techniques for the nondestructive characterization of metallic materials. Nowadays, 3MA is well accepted in industrial production and material research. Over the years, several equipment variants and a wide range of probe heads have been developed, ranging from magnetic microscopes with µm resolution up to large inspection systems for in-line strip steel inspection. 3MA is extremely versatile, as proved by a huge amount of reported applications, such as the quantitative determination of hardness, hardening depth, residual stress, and other material parameters. Today, specialized 3MA systems are available for manual or automated testing of various materials, semi-finished goods, and final products that are made of steel, cast iron, or other ferromagnetic materials. This paper will provide an overview of the historical development, the basic principles, and the main applications of 3MA.
During turning of quenched and tempered AISI4140 surface layer states can be generated, which degrade the lifetime of manufactured parts. Such states may be brittle rehardened layers or tensile residual stresses. A soft sensor concept is presented in this work, in order to identify relevant surface modifications during machining. A crucial part of this concept is the measurement of magnetic characteristics by means of the 3MA-testing (Micromagnetic Multiparameter Microstructure and Stress Analysis). Those measurements correlate with the microstructure of the material, only take a few seconds and can be processed on the machine. This enables a continuous workpiece quality control during machining. However specific problems come with the distant measurement of thin surface layers, which are analyzed here. Furthermore the scope of this work is the in-process-measurement of the tool wear, which is an important input parameter of the thermomechanical surface load. The availability of the current tool wear is to be used for the adaption of the process parameters in order to avoid detrimental surface states. This enables new approaches for a workpiece focused process control, which is of high importance considering the goals of Industry 4.0.
Electromagnetic methods for non-destructive evaluation (NDE) are presented, with which sheet metal components can be identified and their material properties can be characterized. The latter is possible with 3MA, the Micromagnetic Multiparametric Microstructure and stress Analyser. This is a combination of several micromagnetic NDE methods that make it possible to analyse the microstructure in a ferromagnetic material and to determine quantitative values of the mechanical material properties or the stress state. In the case of cold forming, the 3MA application for pre-process testing of sheet metal is discussed. Based on the 3MA information, the formability of the sheets can be predicted. To apply 3MA in-line, the influence of the relative speed and the relative distance between the 3MA probe head and the sheet was investigated. In a second study, a spatially resolved eddy current (EC) method was used to create an image of the intrinsic material microstructure of a component for its identification and traceability. It turned out, that these intrinsic fingerprint images can still be recognized even after subsequent plastic deformation or coating of the surface. This enabled the development of a marker-free traceability method for sheet metal processing. It is based on a low-cost array sensor and a specimen identification using robust and partly redundant features of the fingerprint images processed by machine learning (ML).
The paper addresses the investigation of microstructures from AISI 52100 and AISI 4140 in hardened as well as in quenched and tempered conditions. The specimens are compared in terms of their magnetic hysteresis and their microstructural and mechanical properties. Material properties were determined by hardness, microhardness, and X-ray diffraction measurements. Two different approaches were used to characterize magnetic properties via a hysteresis frame device, aiming, on the one hand, to record the magnetic hysteresis with established proceedings by setting a constant magnetic flux and, on the other hand, by offsetting a constant field strength to facilitate reproducibility of the results with other micromagnetic measurement systems. Comparable differences in both the micromagnetic and the mechanical material properties could be determined and quantified for the specifically manufactured specimens. The sensitivity of the magnetic hysteresis and, determined from that, the relationship between magnetic flux and magnetic field strength were confirmed. It was shown that a consistent change in hysteresis shape from hardened to high temperature tempered material states develops and that this change allows the characterization of different materials without the need to adjust magnetization parameters. Repeatedly, an increase in remanence with decreasing hardness was found for both test approaches. Likewise, a decreasing coercivity and increasing maximum magnetic flux could be detected with decreasing retained austenite content. The investigated correlations should thus contribute to the calibration of comparable measurement systems through the holistic characterized specimens.