The problem of preparing a ternary powder mixture, which was meant to fabricate sintered heterophase composite, and consisted of micro- and two nanosized powders, was analyzed. The microsized powder was a pure magnesium, and as nanocomponents, a silicon powder (nSi) and carbon nanotubes (CNTs) with 2% and 1% volume fractions, respectively, were applied. The powder mixtures were prepared using ultrasonic and mechanical mixing in technological fluid, and four mixing variants were applied. The morphology of the powder mixtures was characterized with scanning electron microscopy (SEM), and then, composite sinters were fabricated in a vacuum with hot temperature pressing at 580 °C under 15 MPa pressure, using a Degussa press. The reaction between the nSi and the Mg matrix, which caused the creation of the Mg₂Si phase in the fabricated Mg-Mg₂Si-CNT composite, was confirmed with X-ray diffraction (XRD). The porosity and hardness of the composite sinters were examined, and optical microscopy (OM) and quantitative image analyses were carried out to characterize the microstructure of the composites. In the manufacturing process of the Mg-nSi-CNT mixtures, the best results were the following: first separate de-agglomeration of nanocomponents, then their common mixing, and finally, the deposition of nanocomponents at the surface of the microsized magnesium powder. The applied procedure ensured the uniform layer formation of de-agglomerated nanocomponents on the Mg powder, without re-agglomerated nSi and CNTs. Moreover, this type of powder mixture morphology allows to obtain sinters with lower porosity and higher hardness, which is accompanied by precipitation of a finer Mg₂Si phase. In the Mg-Mg₂Si-CNT composite, the carbon phase was present, and it was located in the magnesium matrix and in silicide.

Metal matrix composites comprising a magnesium matrix and Mg₂Si/MgO dispersoids obtained by hot pressing silica nanoparticle agglomerates and metal powder in a Degussa press were characterized. Two powder mixtures having weight proportions of Mg:SiO₂ of 10:0.3 and 10:1 were identically sintered. Their microstructures were characterized by optical microscopy and X-ray diffraction. The size and distribution of the Mg₂Si and MgO dispersoids formed in situ were assessed as a function of the original nanosilica content. The behaviour of the composites under compression testing was assessed in 3D by X-ray microtomography using 225kV Nikon X-tek and 150kV Xradia MicroXCT scanners. This provided insights into composite strengthening mechanisms and matrix particle decohesion.

In this study, we present a new composite material that was developed using the pressure infiltration method. In this composite, carbon reinforcement in the form of an open-celled rectangular foam (C_of) was applied, and pure magnesium with two commercial magnesium cast alloys (AZ31, RZ5) was used as the matrix. We examined the microstructure (LM, SEM + EDS) of composites as well as the density, porosity, hardness, compressive strength, flexural strength and tribological properties in dry conditions. It was revealed that the chemical composition of the matrix had a significant impact on the macrostructure, microstructure and properties of the composite. The matrix with rare elements (RZ5) induced poor infiltration of C_of and physicochemical degradation of the reinforcement, while pure magnesium ensured good infiltration, a stable friction coefficient and low wear. For the AZ31 alloy, the effects of infiltration were good; however, an increase in the tribological properties was not observed. Compared with the as-cast matrix materials, the presence of carbon foam in both pure Mg and AZ31 alloy induced an increase in compressive strength and stiffness as well as a decrease in flexural strength. Furthermore, SEM examination of the fractured and wear surfaces microstructure showed structural effects’ dependence on the matrix composition.