Mg matrix in situ composites were fabricated from Mg and ZnO powder by a spark plasma sintering method. The composition and microstructure of the sintered samples were characterized. Corrosion properties of fabricated composites were evaluated by immersion and by electrochemical tests using Hanks’ solution. The results showed that the formation of in situ products improved significantly the corrosion resistance of the fabricated composites compared with pure Mg; Mg-10 wt % ZnO composites especially exhibited the lowest corrosion rate. In addition, an energy-dispersive X-ray (EDX) analysis showed that calcium phosphate formed as a corrosion product on the surface of Mg-10 wt % ZnO composites, while Mg(OH)₂ appeared as a corrosion product on the surface of Mg-20 wt % ZnO composite. The findings suggested Mg-10 wt % ZnO composite as a potential candidate for temporary implant application.

In this study, hydroxyapatite (HAp) coated Mg matrix composites were fabricated for biodegradable implant applications. Spark plasma sintering was employed to fabricate the Mg-10 wt% ZnO composite substrates. HAp was coated on the surface of the sintered composites and pure Mg by a chemical solution treatment. SEM and optical micrographs of coated samples showed that HAp grew homogeneously and formed a layer on the entire surface of both pure sintered Mg and Mg composites. The immersion and polarization test results demonstrated that the HAp coating significantly improved the corrosion resistance of the sintered composites. While the HAp coating layer is not effective in the improvement of the pure Mg substrate, cell culture test results revealed that the HAp coating improved cell adhesion and proliferation on the composites effectively through 72 h, while no cell could survive on the uncoated composites after 72 h. In addition, the corrosion tests and cell culture test results indicated that the composite with longer sintering time has better corrosion resistance and cell viability than those of the composite with shorter sintering time. The findings suggested that the HAp-coated Mg-10 wt% ZnO-2.5 h + 10 min composite is a high-potential candidate for biodegradable implant applications.

Biomedical Mg-matrix in situ composites were fabricated from Mg and ZnO powder via ball mixing and spark plasma sintering. XRD analysis indicated that in situ reactions occurred during sintering process producing MgO, Zn and Mg–Zn intermetallic compounds. The formation of in situ products strongly contributed to the enhancement of the strength and the ductility of the fabricated composites compared with pure Mg. Specifically, the highest strength at 380 MPa was observed in the Mg-20 wt-% ZnO composite, and the highest failure strain at 12.9% was achieved in the Mg-5 wt-% composite compared with the 156 MPa strength and the 10.2% failure strain of pure Mg. In addition, the strengths of as-produced composites are as double as that of cortical bones. With these superior mechanical properties, the fabricated composites are considered as very potential candidate for biomedical load-bearing applications.

In this research, a new space vector modulation control algorithm is proposed to increase the reliability of the cascaded H-bridge multilevel inverters in case of faulty situations, where one or several power cells do not function. Methods to detect faults ensure finding open-circuit module exactly, which is fast and easy to program. By giving a detailed analysis of the impact of the faulty power cells, optimal redundant level states are chosen such that highest possible output voltage can be achieved, while the balance of the three-phase line-to-line voltage is maintained and common-mode voltage is reduced. The proposed algorithm is generalized so that it can be applied to H-bridge inverters of any level. The validity of the method is verified by numerical simulations and experiment results with an 11-level cascaded H-bridge inverter.