The diameter of a micro-tube is very small and its wall thickness is very thin. Thus, when applying double-layer gas-assisted extrusion technology to process a micro-tube, it is necessary to find the suitable inlet gas pressure and a method for forming a stable double gas layer. In this study, a double-layer gas-assisted extrusion experiment is conducted and combined with a numerical simulation made by POLYFLOW to analyze the effect of inlet gas pressure on micro-tube extrusion molding and the rheological properties of the melt under different inlet gas pressures. A method of forming a stable double gas layer is proposed, and its formation mechanism is analyzed. The research shows that when the inlet gas pressure is large, the viscosity on the inner and outer wall surfaces of the melt is very low due to the effects of shear thinning, viscous dissipation, and the compression effect of the melt, so the melt does not easily adhere to the wall surface of the die, and a double gas layer can be formed. When the inlet gas pressure slowly decreases, the effects of shear thinning and viscous dissipation are weakened, but the gas and the melt were constantly displacing each other and reaching a new balanced state and the gas and melt changed rapidly and steadily in the process without sudden changes, so the melt still does not easily adhere to the wall of the die. Thus, in this experiment, we adjusted the inlet gas pressure to 5000 Pa first to ensure that the melt do not adhere to the wall surface and then slowly increased the inlet gas pressure to 10,000 Pa to reduce the viscosity of the melt. Lastly, we slowly decreased the inlet gas pressure to 1000 Pa to form a stable double gas layer. Using this method will not only facilitate the formation of a stable double gas layer, but can also accurately control the diameter of the micro-tube.

Micro-tubes have small diameters and thin wall thicknesses. When using double-layer gas-assisted extrusion (DGAE) technology to process micro-tubes, due to the influence of flow resistance, airflow from the inner gas-assisted layer cannot flow into the atmosphere through the lumen. Over time, it will inflate or even fracture the micro-tubes intermittently and periodically. To solve this problem, a new double-layer micro-tube gas-assisted extrusion die was designed in this study. Its mandrel has an independent airway leading to the lumen of the extrudate, with which the gas flow into the lumen of the extrudate can be regulated by employing forced exhaust. Using the new die, we carried out extrusion experiments and numerical calculations. The results show a significant positive correlation between micro-tube deformation and gas flow rate in the lumen of a micro-tube. Without considering the refrigerant distortion of the microtube, the flow rate of forced exhaust should be set equal to that of the gas from the inner gas-assisted layer flow into the micro-tube lumen. By doing this, the problem of the micro-tube being inflated can be eliminated without causing other problems.

In the process of double-layer gas-assiste extrusion of a plastic micro-tube, the tugging effect caused by the pressure difference of the gas cushion layer inside the die has a great influence on the external dimensions of the micro-tube. Therefore, this study establishes a two-phase extrusion model based on compressible gas and incompressible melt. Ansys Polyflow finite element software was used to numerically simulate the extrusion process of the melt to analyze the effect of the gas cushion layer pressure difference on the micro-tube deformation. The research shows that the shrinkage rate of the micro-tube increases with increasing pressure of the outer cushion layer, and the degree of tube wall migration increases, too. In the process of extrusion, the first normal stress difference at the entrance of the gas cushion layer shows a significant effect on the melt velocity field distribution and the extruded micro-tube cross-sectional deformation.

In the gas-assisted extrusion process, the melt inside the die is in a low-viscosity molten state, so the flow field of the gas cushion layer has a great effect on the cross-sectional shape of the micro-tube. Therefore, this study establishes the gas distribution chamber model of the gas-assisted die. Ansys Fluent software was used to simulate the gas flow field of the gas distribution chamber. The effect of the gas chamber structure on the size of the micro-tube was analyzed by the extrusion experiment. The research shows that the velocity unevenness coefficient of the gas outlet of the single gas chamber die is 11.8%, which is higher than that of the double gas chamber die. The use of a double gas chamber die can improve the stability of the gas cushion layer and the wall thickness non-uniformity of the micro-tube, which verifies the simulation results.