The AlCrN and AlCrON coatings were deposited on plasma nitrided H13 steels through ion-source-enhanced arc ion plating, and their structures, mechanical properties, thermal stabilities, and tribological properties were investigated. Structural analysis showed that the monolayer AlCrN and AlCrON bilayered coatings were mainly composed of fcc-AlCrN and fcc-AlCrON solid solution phases respectively. Upon the addition of thin AlCrON layer, the hardness of AlCrN/AlCrON coating slightly decreased from about 30.5 GPa to 28.6 GPa, and the thermal stability was improved after annealing at 700 °C. Both coatings exhibited excellent wear resistance at room temperature, while all wear process involved a combination of wear mechanisms, including severe abrasion and oxidation at an evaluated temperature. The AlCrON bilayered coating showed better wear resistance than that of AlCrN coating due to a dense anti-oxidation layer and better adhesion at a high temperature, making it suitable for die tool protection coatings.
This study focuses on a comparative analysis of AlCrXN (X = Mo or V) coatings with the reference AlCrN coating via arc ion plating technique (AIP). The XRD and XPS results showed that the AlCrXN coatings were mainly composed of fcc-(Cr,Al)N solid solution phases. Both the AlCrMoN and AlCrVN coatings exhibited much higher hardness and adhesive strength than the AlCrN coating. The addition of Mo or V decreased the coefficient of friction (COF) and wear rate, which was due to the formation of lubricant oxides containing Mo or V on the coating surfaces. The cutting results showed that abrasive wear, adhesive wear, and oxidation wear were the main wear mechanisms for the coated tools at the cutting speeds of 60 m/min and 94 m/min. The addition of Mo or V dramatically improved the cutting performance of AlCrXN-coated tools by increasing the anti-wear ability due to the high hardness and the formed lubricant VOx or MoOx films.
AlCrN/AlCrMoN multilayer coatings with various bilayer numbers (1, 2, 4, and 6) were deposited on high speed steel (HSS) via arc ion plating technology. The effects of bilayer numbers on the microstructure, mechanical and tribological properties were investigated. XRD and TEM results showed that the solid solution (Al, Cr, Mo) N was the main phase in the AlCrN/AlCrMoN multilayer coatings. As compared with the AlCrN/AlCrMoN-1 coating, the AlCrN/AlCrMoN multilayer coatings showed the improved adhesion, hardness and tribology performance. The AlCrN/AlCrMoN-4 coating showed the highest adhesion (Lc2 = 52 N) and micro-hardness (3500 HK0.05). The AlCrN/AlCrMoN-4 coating also exhibited the lowest friction coefficient and wear rate both at room temperature and high temperature due to the optimal structure and good overall performance.
21 April 2025 in Journal of Materials Research and Technology
In this study we examined the effects of compaction pressure for bonding nanocrystalline cemented tungsten carbide (WC-10Co) and high-strength steel (AISI4340) and successfully fabricated a bilayered composite of ceramic and steel. The obtained results were compared with our previous studies, and then the optimised sintering conditions were suggested. The compaction pressure examined varied from 120–200 MPa at 1150°C for 20 min. The study shows that the change in experimental parameters has significant effects on both the sintering properties of nanocrystalline WC-10Co powders and their bonding with AISI4340 steel. The microstructure reveals a successful metallurgical bonding between ceramic and steel. Bonding temperature determines, to a great extent, the diffusion processes across the bonding interface and has found to be the most influential variable compared to sintering time and compaction pressure. The obtained average maximum bonding strength of the bimetal composite is 226 MPa, which is higher than that of previous studies.