Natural fiber composite materials are competent materials that may replace conventional synthetic materials where the strength to weight ratio is essential. In this paper, the mechanical characteristics of composites made up of randomly oriented natural fibers (mudar fiber and snake grass fiber) with nano-silica filler are detailed for the first time. From the various literature surveys, the critical length of mudar and snake grass fiber is chosen as 40 mm and 30 mm, respectively. The test samples were prepared with a fiber content of 10%, 20%, 30%, and 40% with an equal amount of mudar and snake grass fiber. The percentage of nano-filler is maintained as constant as 3% with all the compositions. The composites showed that the highest mechanical properties were found at 30% fiber volume. The maximum tensile strength is 45 MPa, and the flexural strength is 51 MPa. The maximum impact strength is 4.5 J. Sample ID 3 provided the best results compared to other proportions. The fiber/matrix adhesion was investigated using a scanning electron microscope (SEM). These predominant mechanical properties make it easier for the implementation of the prepared composite material in structural and automotive applications.

The selection of fiber is predominant for natural fiber‐reinforced polymer composite materials, which should have easy extraction and good bonding with considerable strength. In this paper, some chemical treatments were done on the fiber material to increase interfacial bonding between the snake grass fiber (Sansevieria ehrenbergii) and polyester matrix, such as alkali treatment (NaOH), potassium permanganate treatment, sodium carbonate treatment, hydrogen peroxide treatment, and calcium carbonate treatment. The chopped snake grass fiber‐reinforced polymer composite material was prepared by keeping 25 wt.% of fiber and 30 mm fiber length reinforced with an unsaturated polyester resin that was cured with the help of the catalyst methyl ethyl ketone peroxide (MEPK). Cobalt naphthenate was used as an accelerator. Tribological properties were discussed for the highly potential sample with the help of a pin‐on‐disc wear tester, and the results were analysed by the Taguchi L9 orthogonal array. This paper exhibited the best mechanical and tribological properties among those chemical‐treated fibers used in fiber‐reinforced composite materials and untreated fibers used in fiber‐reinforced composite materials. CaCO₃ treatment provided higher tensile strength (45 MPa), impact strength (3.35 J), and hardness (27 BHN). Finally, the mechanical and tribological characterization of the samples was done with the aid of SEM (scanning electron microscope).