Evaluation of creep compliance of particulate composites using empirical models always provides parameters depending on initial stress and material composition. The effort spent to connect model parameters with physical properties has not resulted in success yet. Further, during the creep, delamination between matrix and filler may occur depending on time and initial stress, reducing an interface adhesion and load transfer to filler particles. In this paper, the creep compliance curves of glass beads reinforced poly(butylene terephthalate) composites were fitted with Burgers and Findley models providing different sets of time-dependent model parameters for each initial stress. Despite the finding that the Findley model performs well in a primary creep, the Burgers model is more suitable if secondary creep comes into play; they allow only for a qualitative prediction of creep behavior because the interface adhesion and its time dependency is an implicit, hidden parameter. As Young’s modulus is a parameter of these models (and the majority of other creep models), it was selected to be introduced as a filler content-dependent parameter with the help of the cube in cube elementary volume approach of Paul. The analysis led to the time-dependent creep compliance that depends only on the time-dependent creep of the matrix and the normalized particle distance (or the filler volume content), and it allowed accounting for the adhesion effect. Comparison with the experimental data confirmed that the elementary volume-based creep compliance function can be used to predict the realistic creep behavior of particulate composites.
Auxetic metamaterials exhibit unique mechanical behavior due to their negative Poisson’s ratio, but reliable determination of their effective elastic properties remains challenging. In this study, an experimental–numerical approach is proposed to characterize additively manufactured polylactic acid (PLA)-based auxetic sandwich structures. Material properties were first assessed using tensile testing, melt flow rate/volume rate (MFR/MVR) measurements, Fourier-transform infrared (FTIR) spectroscopy, differential scanning calorimetry (DSC), dilatometry, and nanoindentation, revealing stable mechanical behavior, good processability, and slight increases in crystallinity induced by the printing process. Impulse excitation technique (IET) measurements provided highly reproducible resonant frequencies, demonstrating a strong dependence on core geometry and orientation. However, classical ASTM-based evaluation yielded non-physical elastic properties, highlighting its limitations for architected metamaterials. Finite element modal analyses, combined with inverse parameter identification, enabled the determination of effective elastic properties using a transversely isotropic homogenized model. This approach significantly improved the agreement between experimental and numerical results. The findings revealed pronounced anisotropy and orientation-dependent auxetic behavior, including a negative Poisson’s ratio for specific configurations. The proposed methodology provides a suitable framework for the reliable characterization and design of complex metamaterials.