Carbon neutrality has led to a surge in the popularity of hydrogen tanks in recent years. However, designing high-performance tanks necessitates the precise determination of input material properties. Unfortunately, conventional characterization methods often underestimate these material properties. To address this limitation, the current research introduces alternative designs of ring tensile specimens, which enable accurate and reliable characterization of filament-wound structures. The advantages and disadvantages of these alternative designs are thoroughly discussed, considering both numerical simulations and experimental investigations. Moreover, the proposed ring tensile methods are applied to characterize thermoplastic composites for hydrogen storage tanks. The results indicate that the mechanical strengths and stiffness of carbon fiber-reinforced thermoplastic Elium® 591 composites closely match those of epoxy-based composites. This newfound accuracy in measurement is expected to contribute significantly to the development of recyclable hydrogen tanks.
This study presents a methodology for characterizing the constituent properties of composite materials by back-calculating from the laminate behavior under fatigue loading. Composite materials consist of fiber reinforcements and a polymer matrix, with the fatigue performance of the laminate governed by the interaction between these constituents. Due to the challenges in directly measuring the properties of individual fibers and the polymer matrix, a reverse-engineering approach was employed. Using the micro-mechanics of fatigue (MMFatigue), we predicted the laminate’s fatigue behavior based on assumed constituent properties and compared these predictions with experimental data from fatigue tests. The properties of the fiber and polymer matrix were iteratively adjusted to minimize the differences between predictions and experimental results, enabling accurate fatigue characterization. To ensure robustness, three laminate angles—0°, 30°, and 60°—were evaluated at three temperatures: low temperature (LT: −40 °C), room temperature (RT: 25 °C), and high temperature (HT: 85 °C). The error, defined as the fatigue life difference between the prediction and the experimental results, were obtained as 2.48% at LT, 7.18% at RT, and 1.25% at HT for a laminate angle of 45°. Finally, the applicability of the multiscale-based fatigue life prediction method was demonstrated through studies on laminates with various angles under tension–compression, and compression–compression cyclic loads, as well as composite pressure vessels under cyclic loading.
As large-scale additive manufacturing advances, the reliable prediction of the structural behavior of FDM-printed composites is becoming increasingly important. However, existing finite element methods often oversimplify the material anisotropy introduced by the printing path. This study proposes a projection-based method that maps toolpath-defined fiber orientations directly into a finite element model to represent anisotropic mechanical behavior. The mechanical properties of printed carbon fiber-reinforced ABS were experimentally characterized in three directions (UDL, UDT, and UD10). The results confirmed strong anisotropy, with elastic moduli ranging from 3.2 to 9.8 GPa and tensile strengths from 20 to 81 MPa. The shear modulus and strength obtained from the 10° off-axis tensile tests were 1.17 GPa and 10.9 MPa, respectively. This directional data enabled the implementation of the FE model of a 20 m-long printed ship structure. The predicted mid-span deflection (2.19 mm) differed by only 5% from the experimental measurement (2.08 mm). While effective, this method may face challenges with highly irregular geometries. Nevertheless, it offers a scalable approach for the accurate simulation of FDM-printed composites.