Laser-powder bed fusion (LPBF) is one of the preferred techniques for producing Co-Cr metal structures for dental prosthodontic appliances. However, there is generally insufficient information about material properties related to the production process and parameters. This study was conducted on samples produced from three different commercially available Co-Cr dental alloys produced on three different LPBF machines. Identically prepared samples were used for tensile, three-point bending, and toughness tests. Light microscopy (LM), scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD) analyses of microstructure were performed after testing. Differences were observed in microstructures, which reflected statistically significant differences in mechanical properties (one-way analysis of variance (ANOVA) and Scheffé post hoc test (α = 0.05)). The material produced on the 3D Systems DMP Dental 100 had 24 times greater elongation ε than the material produced on the Sysma MySint 100 device and the EOS M100 machine. On the other hand, the material produced on the EOS M100 had significantly higher hardness (HV0.2) than the other two produced materials. However, the microstructure of the Sysma specimens with its morphology deviates considerably from the studied group. LPBF-prepared Co-Cr dental alloys demonstrated significant differences in their microstructures and, consequently, mechanical properties.
This paper investigates the casting defects of a stainless steel pump impeller manufactured through the sand casting process. The material characterization of austenitic steel AISI 316L was initially carried out, which examined the chemical composition of the casting and its microstructure. The next step was to determine the cause of the casting defects using numerical simulations. The numerical simulations were performed using ProCAST software (Version 18.0). Initial results of the filling and solidification simulations were conducted using the parameters employed in the actual casting process, revealing casting defects in corresponding locations. The casting process was subsequently modified to achieve improved results. This involved reconstructing the gating system, redesigning the riser, and incorporating a cylindrical chiller. The results show that the modified casting process significantly reduces the occurrence of defects in the final product. The study provides useful insights into the analysis and modification of the casting process for stainless steel pump impellers produced through sand casting. The results can help improve the quality of such products and reduce production costs associated with casting defects.
Silanized glass fibers are popular reinforcements of acrylic denture base materials. To increase the number of surface hydroxyl groups and to improve interfacial adhesion between the matrix and reinforcements, acid or base treatments of glass fibers are commonly performed before the silanization. However, limited data are available on the effect of these treatments on the mechanical properties of acrylic matrix composite materials used for denture base applications. In this work, before the silanization of a woven glass fiber fabric (GF) with 3-(trimethoxysilyl) propyl methacrylate, activation pretreatments using HCl and NH4OH aqueous solutions have been performed. To characterize the glass surface, FTIR spectroscopy was used. Specimens of cured acrylic denture base resin and composites were divided into five groups: (1) cured acrylic denture base resin-control group; (2) composite with non-silanized GF; (3) composite with silanized GF; (4) composite with NH4OH activated and silanized GF; (5) composite with HCl activated and silanized GF. The flexural and impact properties of specimens were evaluated by means of three-point-bending tests and Charpy impact testing, respectively. The residual reactivity of the samples was analyzed using differential scanning calorimetry. The results of mechanical testing showed that acid and base pretreatments of the glass fabric had a positive effect on the flexural modulus of prepared composites but a negative effect on their impact strength. Possible interfacial adhesion mechanisms and the diffusion control of isothermal cure reactions due to vitrification have been discussed.
This research explores how variations in laser powder bed fusion (LPBF) parameters—laser power (P), scanning speed (v), and base plate preheating temperature (ϑp)—affect the mechanical properties of the EOS Co-Cr SP2 dental alloy. A central composite design (CCD) was used to optimize the process parameters. Mechanical testing focused on crucial properties for dental applications, including yield strength (Rp0.2), elongation (ε), toughness (KVa), and flexural strength (Rms). Microstructural analysis was conducted using light and electron microscopy, while XRD identified microstructural phases. Statistical analysis (ANOVA, Scheffé post hoc test, α = 0.05) revealed significant effects of P, v, and ϑp on the mechanical properties. Response surface models (RSMs) were developed, and optimal parameters were determined to achieve maximum toughness and flexural strength. Maximum values were obtained with laser power above 205 W and base plate preheating at 310 °C. The mathematical model predicted toughness values with less than 5% deviation from experimental results, indicating high accuracy.
High speed steel (HSS) is a very important industrial tool material and has been constantly improved for different wear resistance applications and cutting tools, i.e. drills, milling cutters, hobs and for the cutting tools in which the economical cutting speed is too low for choosing the carbide tools. The properties of HSS depend significantly on the parameters of the conducted heat treatment. In this paper, the influence of deep cryogenic treatment in combination with nitriding of metallurgical powder metallurgy HSS on the wear resistance was measured. Additionally, the cutting performance in a single point cutting tool machinability test at the configuration of the dry low-speed turning of steel was investigated. The results showed that deep cryogenic treatment itself, and in combination with nitriding, resulted in the reduction of the wear rate. The results of the single point cutting tool machinability test showed that deep cryogenic treated and nitrided HSS inserts performed worse than the classically heat-treated inserts and deep cryogenic treated HSS inserts exhibited approximately the same flank wear as the nitrided ones.
This paper explores the influence of graphite shape, type, and dimensions on the thermal characteristics of Fe-C cast iron. Test samples were prepared from blocks of grey and nodular cast iron, specifically examining castings with D and A types of graphite as well as nodular graphite in a ferrite matrix. To analyze the effect of surface texture, sample surfaces were prepared with varying parameters of surface roughness, achieving values of 0.5 μm for polished and 12.6 μm for unpolished surfaces. Thermal characteristics, including thermal conductivity and effusivity, were evaluated using unsteady hot disk methods, with water as the contact agent, to simulate practical thermal conditions. Additionally, the microstructure of each sample was analyzed using optical microscopy. Results indicate that graphite content, type, shape, and surface roughness collectively have the most significant impact on the thermal properties of cast iron. This study’s findings provide valuable insights into optimizing cast iron for applications requiring efficient thermal management and highlight the importance of graphite morphology and surface finish in enhancing thermal performance.