Aluminum tris-(diethylphosphinate) (AlPi) is known to have an efficient flame-retardant effect when used in poly(butadiene terephthalates) (PBT). Additionally, better flame-retardant effects can be achieved through the partial substitution of AlPi by boehmite in multi-component systems, which have been shown to be an effective synergist due to cooling effects and residue formation. Although the potential of beneficial effects is generally well known, the influence of particle sizes and behavior in synergistic compositions are still unknown. Within this paper, it is shown that the synergistic effects in flammability measured by limiting oxygen index (LOI) can vary depending on the particle size distribution used in PBT. In conducting thermogravimetric analysis (TGA) measurements, it was observed that smaller boehmite particles result in slightly increased char yields, most probably due to increased reactivity of the metal oxides formed, and they react slightly earlier than larger boehmite particles. This leads to an earlier release of water into the system enhancing the hydrolysis of PBT. Supported by Fourier transformation infrared spectroscopy (FTIR), we propose that the later reactions of the larger boehmite particles decrease the portion of highly flammable tetrahydrofuran in the gas phase within early burning stages. Therefore, the LOI index increased by 4 vol.% when lager boehmite particles were used for the synergistic mixture.

The production of components consisting of various polymer types by welding is severely restricted and only possible for bonding compatible materials with melting points in a close range. Several modifications, such as the cross-linking of one joining partner, allow for circumventing the restrictions regarding the melting points but do not help in joining bonding incompatible materials. Investigations of dissimilar material combinations, especially from polymer-metal hybrid structures, show a high potential of connections based on form fits. Within the scope of this paper, the possibility of joining incompatible polymer combinations, such as polyamide 66 and high-density polyethylene, by micro form fit using the vibration welding process is analyzed. For this purpose, the generated bonding strength of the test specimen was determined by shear tests. Furthermore, the undercuts of the generated prestructures and the resulting bond of the test specimen were examined microscopically by computer-tomography. These investigations depict the high potential of joining incompatible polymer combinations by form fit in the vibration welding using prestructuring to generate undercuts.

The wear behaviour of PBT-steel gear sets under temporarily changed load has been investigated using an in situ gear test rig developed at the LKT. The in situ test method is based on analysing the timing differences between the index pulses of rotary encoders on the input and output shaft of the test rig. The loading torque was varied between two levels and compared to the permanently applied equivalent average load in terms of the resulting tooth flank wear. Moreover, the number of load changes has been varied to analyse the influence of load changes on the gear wear. The results show that the applied load spectrum determines the resulting tooth flank wear even if the average applied load is the same. Moreover, it could be shown that the sequence of the applied load, i.e., the load history, plays an important role, since the applied load and the duration of the applied load within the run-in-stage disproportionately affect the wear behaviour over time.

Laser‐sintering offers the possibility to produce complex and individualized components cost‐effectively. To fully exploit the advantages of laser‐sintering in assemblies with mass‐produced components, high‐performance joining processes like welding are necessary. Thus, a cost‐effective customization of products can be enabled, which allows to follow the increasing trend of individualization. Infrared welding, in particular, can also be suitable for complex laser‐sintered parts due to the reduced transverse forces during joining, compared to other welding processes. The investigations show that high strength between PA12 laser‐sintered and injection‐molded components can be achieved by infrared welding. The bond strength is mainly influenced by the welding parameters. Especially a low weld pressure leads to high achievable strengths and failure outside the weld seam. Joints between laser‐sintered parts and glass fiber reinforced injection‐molded components demonstrate the transferability of the obtained knowledge. The residual melt layer thickness of the joint decreases with increasing weld pressure, as the morphological characterization shows. Besides, the typical morphological seam structure can be seen on the side of the injection‐molded component. In the area of the laser‐sintered components, a deviating morphological structure can be observed. Distinctive flow lines can be observed, spherulitic structures can only partially be seen as well as deformed spherulites.