Laser irradiation is a popular method to produce microtextures on metal surfaces. However, the common laser-produced microtextures were hierarchical (multiscale), which may limit their applicability. In this paper, a method of two-step laser irradiation, combining first-step strong ablation and sequentially second-step gentle ablation, was presented to produce micron-rough surface with single-scale microtextures. The effect of laser fluence on the Ti–6Al–4V surface morphology and wettability were investigated in detail. The morphology results revealed that the microtextures produced using this method gradually evolved from multiscale to single-scale meanwhile from microprotrusions to microholes with increasing the second-step laser fluence from 0.0 to 2.4 J/cm2. The wettability and EDS/XPS results indicated that attributing to the rich TiO2 content and micron roughness produced by laser irradiation, all the two-step laser-irradiated surfaces exhibited superhydrophilicity. In addition, after silanization, all these superhydrophilic surfaces immediately turned to be superhydrophobic with close water contact angles of 155–162°. However, due to the absence of nanotextures, the water-rolling angle on the superhydrophobic surfaces with single-scale microtextures distinctly larger than those with multiscale ones. Finally, using the two-step laser-irradiation method and assisted with silanization, multifunctional superhydrophobic Ti–6Al–4V surfaces were achieved, including self-cleaning, guiding of the water-rolling direction and anisotropic water-rolling angles (like the rice-leaf), etc.
Ultrasonic vibration (UV) is widely used in the forming, joining, machining process, etc. for the acoustic softening effect. For parts with small dimensions, UV with limited output energy is very suitable for the microforming process and has been gaininf more and more attention. In this investigation, UV-assisted uniaxial tensile experiments were carried out utilizing GB 5052 thin sheets of different thicknesses and grain sizes, respectively. The coupling effects of UV and the specimen dimension on the properties of the material were analyzed from the viewpoint of acoustic energy in activating dislocations. A reduction of flow stress was found for the existing acoustic softening effects of UV. Additionally, the residual effects of UV were demonstrated when UV was turned off. The uniform deformation ability of thin sheet could be improved by increasing the hardening exponent with UV. The experimental results indicate that UV is very helpful in improving the forming limit in microsheet forming, e.g., microbulging and deep drawing processes.