Bacterial cellulose (BC) is a natural polymer with properties suitable for tissue engineering and possible applications in scaffold production. However, current procedures have limitations in obtaining BC pellicles with the desired structural, physical, and mechanical properties. Thus, this study analyzed the optimal culture conditions of BC membranes and two types of processing: draining and oven-drying. The aim was to obtain BC membranes with properties suitable for a wound dressing material. Two studies were carried out. In the preliminary study, the medium (100 mL) was inoculated with varying volumes (1, 2, 3, 4, and 5 mL) and incubated statically for different periods (3, 6, 9, 12, and 18 days), using a full factorial experimental design. Thickness, uniformity, weight, and yield were evaluated. In the optimization study, a Box–Behnken design was used. Two independent variables were used: inoculum volume (X₁: 1, 3, and 5 mL) and fermentation period (X₂: 6, 12, and 18 d) to determine the target response variables: thickness, swelling ratio, drug release, fiber diameter, tensile strength, and Young’s modulus for both dry and moist BC membranes. The mathematical modelling of the effect of the two independent variables was performed by response surface methodology (RSM). The obtained models were validated with new experimental values and confirmed for all tested properties, except Young’s modulus of oven-dried BC. Thus, the optimal properties in terms of a scaffold material of the moist BC were obtained with an inoculum volume of 5% (v/v) and 16 d of fermentation. While, for the oven-dried membranes, optimal properties were obtained with a 4% (v/v) and 14 d of fermentation.

The tribological performance of Glass Fiber Reinforced Polymer (GFRP) composites is essential for applications in automotive, aerospace, and industrial sectors. This study investigates the effect of fiber weight fraction ratio (wf.) (50%, 65%, and 70%), applied load, and sliding speed on the tribological behavior of twill-woven GFRP using a pin-on-disc tribometer. Experimental trials were carried out to assess the impact of control factors on the coefficient of friction, specific wear rate, and contact temperature. Statistical analyses based on generalized linear models (GLM) method or multi-factor ANOVA, identified the most significant factors and their contributions. Results indicate that sliding speed contributes the highest to COF (46.51%), while fiber wf. primarily influences wear rate (34.15%). The applied load was found to have the strongest impact on contact temperature (39.08%). Furthermore, SEM and EDS analyses reveal dominant wear mechanisms, including abrasive wear and transfer layer formation. This study introduces the novelty of using statistical modeling to optimize GFRP for high-performance tribological applications, providing a more precise and efficient approach to enhancing their properties.

This paper presents three methods of converting complex 3D models of STL type into solid models. For converting the STL models, specific approximation functions from CATIA and Creo Parametric software were used as well as 3D solid modeling methods that used sketches drawn for sections of the specific analyzed model. This conversion is required to get a solid 3D model that can be used for finite element analysis and to be processed using Boolean functions in specific CAD programs. This paper also presents a study of the effectiveness of FEA in respect to the time required for the analysis of each converted model. The analyzed STL files contain data obtained by computer tomography and are the 3D models of the human orthopedic system: the left zygomatic bone and upper part of the right femur. The presented conversion methods can be used by design engineers both in medical applications (where the complexity of forms is well known) for the design of implants and for industrial applications for reverse engineering.

Calcium nitrate is considered a promising accelerator in cement-based composites, with high potential in 3D printing and cold cement concreting. The effect induced by the composition of calcium nitrate tetrahydrate (CN) accelerator into white Portland cement is evaluated here from three perspectives: (1) Fresh cement paste properties in terms of setting time and slump, (2) mechanical properties of hardened cement samples at 7 and 28 days and (3) material characteristics in terms of structure and porosity that further link the presence of the accelerator with the macroscopic performances. The compressive and flexural strength of the hardened samples, evaluated after 7 and 28 days of hydration, indicate a non-monotonous trend with CN concentration. Crystalline phase composition is investigated using X-ray diffraction (XRD). The morphology and texture are analyzed at the flexure interface by visual inspection and electron microscopy. Complementary, the porous features are investigated by NMR-relaxometry on dry and cyclohexane-filled samples. The studies confirm that CN promotes changes in the composition and morphology of hydrates, while a trend of increase in capillary porosity is outlined as well. This competition between multiscale effects may be quantified by NMR and complementary techniques to further clarify the mechanical behavior of such composites.

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