The aim of this study is to investigate the impact of time and temperature of the heat pump drying process of soursop slices at different levels on moisture content and total polyphenol content (TPC). Twelve types of classical kinetic models have been used in this work to describe the suitability of experimental data with models. The conformity is assessed based on statistical values (e.g., coefficient of determination (R2), Chi–square value (X2), etc.). The loss of moisture in the material is described in accordance with Fick’s diffusion law. Value of moisture rate (MR), and effective moisture diffusivities (Deff) have been identified. Experimental results show that MR value depends on the time and drying temperature, Deff increases when increasing the drying temperature from 20–50 °C with values of 1.24 × 10−9, 1.85 × 10−8, 7.69 × 10−8, and 5.54 × 10−7 m/s2. The Singh et al. model is the best option to describe the moisture of the sliced soursop drying process at 30 °C (R2 = 0.97815). The largest TPC decomposition occurs at a temperature of 50 °C. The ability to decompose TPC is proportional to the drying temperature. The TPC decomposition dynamic model follows a first–order reaction when drying at 20 °C with a determinant coefficient R2 = 0.9693.
Co-doped Fe-MOF bimetallic organic framework materials at different ratios were synthesized based on the solvothermal method, and we evaluated their morphological characteristics by modern analytical methods such as SEM, XRD, FT-IR, and isotherm of nitrogen adsorption-desorption (BET). The specific surface area of the 0.3 CoFe-MOF sample (280.9 m2/g) is much larger than the Fe-MOF and samples at other ratios. The post-synthesized materials were evaluated for their ability to absorb various dyes, including Methylene Blue (MB), Methyl orange (MO), Congo red (CR), and Rhodamine (RhB), and evaluated for the effects of pH, the initial concentration of the dye solution, time, and dose of adsorbent. The results show that the 0.3 CoFe-MOF material has a high adsorption capacity that is superior to both the original Fe-MOF and the CoFe-MOFs at other ratios. The highest adsorption capacity of MB dye by 0.3 CoFe-MOF reaches up to 562.1 mg/g at pH 10, the initial concentration of MB of 200 mg/L, after 90 min. The charged properties of the dyes and the charged nature of the bimetallic organic frameworks are best demonstrated through the adsorption of dye mixtures. The adsorption efficiency on the mixed system of cationic (MB) and anionic (MO) dyes yielded the highest removal efficiency of 70% and 81%, respectively, after 30 min. Therefore, the research has opened up the potential application of M/Fe-MOF modified materials and CoFe-MOF in organic dyes adsorption in wastewater treatment for environmental protection.
Imidacloprid, acephate, and carbaryl are common insecticides that are extensively used in planting mango, a well-known fruit in Vietnam, to ease mango hopper issues. The accurate detection of pesticide residues is critical for mango export to meet quality criteria. This study developed a novel SERS platform by using polydimethylsiloxane (PDMS) to simulate the rose petal structure incorporated with a silver coating layer and silver nanoparticles (AgNPs) to detect imidacloprid, acephate, and carbaryl in mango fruits. In this paper, the rose petal PDMS/Ag-AgNPs replica was considered the most efficient substrate for SERS measurement with an EF of 4.7 × 107. The Raman spectra of the three insecticides obtained from the PDMS/Ag-AgNPs substrate were clearly observed with their characteristic peaks of 1105 cm−1 for imidacloprid, 1083 cm−1, and 1579 cm−1 for acephate, and 727 cm−1 and 1378 cm−1 for carbaryl. The application of PDMS/Ag-AgNPs substrate in quantitative analysis of the three pesticides in mango fruit was evaluated. As a result, the limit of detection was 0.02 mg/kg for imidacloprid, 5 × 10−5 mg/kg for acephate, and 5 × 10−3 mg/kg for carbaryl. The SERS result also revealed that the pesticide residues in the mango sample were within an acceptable limit. This suggested the possibility of the rose petal PDMS/Ag-AgNPs replica for rapid quantification of pesticide residues not only in mango fruit but also in many other agricultural products.
Honey is a natural product made by honeybees, its composition depends on factors such as climate, soil and plant source. In this study, the nutritional parameters, phenolic composition, antioxidant activity and antibacterial ability of 30 different types of honey of different botanical and geographical origins in Vietnam were investigated. The study focused on the characterization and evaluation of the influence of plant origin and geographical location on physical–chemical properties and biological activities (antioxidant and antibacterial). The obtained results show that all honey samples meet quality standards according to international standards and Vietnamese standards, except for some exceptions recorded in moisture, 5-hydroxymethylfurfural (HMF) value and ash. These samples were explored for the detection of 13 polyphenols by using high-performance liquid chromatography (HPLC). The classification of honey samples collected from different regions and botanical sources was performed by principal component analysis (PCA), and it was observed that certain phenolic compounds contributed to the identification of honey samples. In addition, the correlation between physicochemical properties, chemical composition and biological activity of most honeys was also first clarified in this study. Overall, our data provide an overview data set and essential results in creating a database on the world honey trait map.
Free fatty acids (FFAs) were obtained from hydrolyzed virgin coconut oil (VCO) by Candida rugosa lipase (CRL). Four factors’ influence on hydrolysis degree (HD) was examined. The best hydrolysis conditions in order to get the highest HD value were determined at VCO to buffer ratio 1 : 5 (w/w), CRL concentration 1.5% (w/w oil), pH 7, and temperature 40°C. After 16 hours’ reaction, the HD value achieved 79.64%. FFAs and residual hydrolyzed virgin coconut oil (HVCO) were isolated from the hydrolysis products. They were tested for their antibacterial activity against Gram-negative and Gram-positive bacteria, which can be found in contaminated food and cause food poisoning. FFAs showed their inhibition against Bacillus subtilis (ATCC 11774), Escherichia coli (ATCC 25922), Salmonella enteritidis (ATCC 13076), and Staphylococcus aureus (ATCC 25923) at minimum inhibitory concentration (MIC) of 50%, 60%, 20%, and 40%, respectively. However, VCO and HVCO did not show their antibacterial activity against these tested bacteria.
About Me
Institute of Applied Technology and Sustainable Development, Nguyen Tat Thanh University, Ho Chi Minh City 700000
Institute of Applied Technology and Sustainable Development, Nguyen Tat Thanh University, Ho Chi Minh City 700000