The effects of heat treatments on microstructure and basic mechanical properties of selective laser melted (SLM) TC4 titanium alloy were investigated in detail. The results demonstrated that a lot of acicular α/α′ and β phases exist in the SLM TC4 titanium alloy. With the increase in the aging treatment temperature, the metastable α′ phase of SLM TC4 was decomposed into α + β laths. Moreover, the α/α′ phase and β phase grew coarser, leading to a gradual decrease in strength, that is, plasticity and hardness increased and decreased, respectively. In terms of solid-solution aging treatment, the β phase was transformed into the α′ martensite phase in the solid-solution treatment, and the aging treatment induced the decomposition of the metastable α′ phase into α + β laths. The strength and hardness of SLM TC4 alloy increased as the temperature increased. The optimal mechanical properties could be obtained by water quenching after holding at 960 ℃ for 1 h and then air cooling after holding at 600 °C for 8 h.
The uniaxial tensile behavior of MarBN steel with a constant strain rate of 5 × 10−5 s−1 under various temperatures ranging from room temperature to 630 °C was analyzed. This study aimed to identify the effect of the temperature on the tensile behavior and to understand the microstructure deformation by electron backscatter diffraction. The tensile results showed that the yield and ultimate tensile strength decreased with increasing temperature. Serrated flow was observed from 430 °C to 630 °C. The electron backscatter diffraction analysis showed that the low-angle grain boundaries decreased at the medium deformation and increased at the maximum deformation. In contrast, they decreased with increasing temperatures. In addition, the number of voids increased with the increasing plastic strain. As the strain increased, the voids joined together, and the tiny cracks became larger and failed. Three mechanisms were responsible for the tensile deformation failure at various temperatures: grain rotation, the formation and rearrangement of low angle grain boundaries, and void nucleation and propagation. Finally, the formation of the low-angle grain boundaries and voids under different degrees of deformation is discussed.
The effect of strain rate and temperature on the thermomechanical behavior and microstructure of MarBN steel is studied with the strain rates of 5 × 10−3 and 5 × 10−5 s−1 from room temperature (RT) to 630 °C. At high strain rates of 5 × 10−3 s−1, the Holloman and Ludwigson equations can better predict tensile plastic properties. In contrast, under low strain rates of 5 × 10−5 s−1, coupling of the Voce and Ludwigson equations appears to predict the flow relationship at RT, 430, and 630 °C. However, the deformation microstructures have the same evolution behavior under strain rates and temperatures. Geometrically necessary dislocations appear along the grain boundaries and increase the dislocation density, which results in the formation of the low-angle grain boundaries and a decrease in the number of twinning. The strengthening sources of MarBN steel include grain boundary strengthening, dislocation interactions, and multiplication. The fitted R2 values of these models (JC, KHL, PB, VA, ZA) to plastic flow stress at 5 × 10−5 s−1 are greater than 5 × 10−3 s−1 for MarBN steel. Due to the flexibility and minimum fitting parameters, the phenomenological models of JC (RT and 430 °C) and KHL (630 °C) give the best prediction accuracy under both strain rates.
To reduce harmful gas emission and improve the operational efficiency, advanced ultra-supercritical power plants put forward higher requirements on the high temperature mechanical properties of applied materials. In this paper, the tensile behavior and deformation mechanisms of MarBN steel are discussed at different strain rates (5 × 10−3 s−1, 5 × 10−4 s−1, and 5 × 10−5 s−1) under room temperature and 630 °C. The results show that the tensile behavior of the alloy is dependent on temperature and strain rate, which derived from the balance between the average dislocation velocity and dislocation density. Furthermore, observed dynamic recrystallized grains under severe deformation reveal the existence of dynamic recovery at 630 °C, which increases the elongation compared to room temperature. Finally, three typical constitutive equations are used to quantitatively describe the tensile deformation behavior of MarBN steel under different strain rates and temperatures. Meanwhile, the constitutive model of flow stress for MarBN steel is developed based on the hyperbolic sine law.