When laser cladding is used to repair parts, the interaction of parameters has a significant influence on equipment performance. In order to explore the process parameters and quality of Ni60PTA coating, the statistical relationship between the process parameters (laser power, scanning speed, and powder feeding rate) and the responses (dilution ratio, ratio of layer width to height, and contact angle) was established by experiments using the response surface method (RSM) and variance analysis. The results show that the laser power is the dominant factor affecting the dilution ratio. However, the scanning speed has the greatest influence on the ratio of layer width to height and contact angle. These experimental results show that the proposed model can predict the actual data. In addition, the microstructure and microhardness of the samples prepared with the optimum process parameters were characterized. The results show that the quality of the cladding layer is good without cracks, deformation, and pores. The microstructure of the cladding zone is mainly composed of γ (Ni), FeNi3, M (M = Fe, Ni, Cr)23C6, M7C3, and CrB. The average microhardness of the coating is about 620 HV0.2, which is about 3.1 times that of 45 steel substrate.
In order to extend the service life of 45# steel and reduce production costs, coating NiCrBSi alloy powder on the surface of 45# steel can meet production requirements, avoid resource waste and achieve green manufacturing. Based on response surface method (RSM), the dilution rate, aspect ratio and contact angle were taken as the optimization goals, and the process parameters (laser power, scanning speed and powder feeding rate) were optimized and the optimal process parameters were determined. On this basis, the microstructure of Ni-based coating was characterized by the cladding experiment. The friction wear and corrosion resistance of the coating were tested, and the enhancement mechanism of the wear resistance and corrosion resistance of the coating was analyzed. The results show that the optimized coating has good corrosion resistance and wear resistance. It provides a reference for the optimization of process parameters in 45# steel repair work.
Intermetallic compounds have been studied for their potential application as structural wear materials or coatings on engineering steels. In the present work, a newly designed intermetallic composite in a Ni–Mo–Si system was fabricated by arc-melting process with commercially pure metal powders as starting materials. The chemical composition of this intermetallic composite is 45Ni–40Mo–15Si (at %), selected according to the ternary alloy diagram. The microstructure was characterized using optical microscopy (OM), scanning electron microscopy (SEM), X-ray diffraction (XRD), and energy dispersive spectroscopy (EDS), and the wear-resistant properties at room temperature were evaluated under different wear test conditions. Microstructure characterization showed that the composite has a dense and uniform microstructure. XRD results showed that the intermetallic composite is constituted by a binary intermetallic compound NiMo and a ternary Mo2Ni3Si metal silicide phase. Wear test results indicated that the intermetallic composite has an excellent wear-resistance at room-temperature, which is attributed to the high hardness and strong atomic bonding of constituent phases NiMo and Mo2Ni3Si.
14 October 2023 in The International Journal of Advanced Manufacturing Technology
Intermetallic compounds are increasingly being expected to be utilized in tribological environments, but to date their implementation is hindered by insufficient ductility at low and medium temperatures. This paper presents a novel multiphase intermetallic alloy with the chemical composition of Mo–40Ni–13Si (at %). Microstructure characterization reveals that a certain amount of ductile Mo phases formed during the solidification process of a ternary Mo–Ni–Si molten alloy, which is beneficial to the improvement of ductility of intermetallic alloys. Tribological properties of the designed alloy—including wear resistance, friction coefficient, and metallic tribological compatibility—were evaluated under dry sliding wear test conditions at room temperature. Results suggest that the multiphase alloy possesses an excellent tribological property, which is attributed to unique microstructural features and thereby a good combination in hardness and ductility. The corresponding wear mechanism is explained by observing the worn surface, subsurface, and wear debris of the alloy, which was found to be soft abrasive wear.
Intermetallic compounds are increasingly being expected to utilize in tribological environments, but to date the works are hindered by insufficient ductility at low and medium temperature. This paper presents a novel multiphase intermetallic alloy with the chemical composition of Mo-40Ni-13Si (at.%). Microstructure characterization reveals that a certain amount of ductile Mo phases formed during the solidification process of ternary Mo-Ni-Si alloy melt, which is undoubtedly beneficial to the ductility improvement of intermetallic alloy. Tribological properties of the designed alloy, including wear resistance, friction coefficient and metallic tribological compatibility, were evaluated under dry sliding wear test conditions at room temperature. Results suggested that the multiphase alloy possesses an excellent property for room-temperature wear applications, which is attributed to the unique microstructural features and thereby good combination in hardness and ductility. The corresponding wear mechanism is also reported by observing the worn surface, subsurface and wear debris of alloy, which to be found is soft abrasive wear.