Few systematic studies on the correlation between alloy microstructure and mechanical failure of the AlSi10Mg alloy produced by laser-based powder bed fusion (L-PBF) are available in the literature. This work investigates the fracture mechanisms of the L-PBF AlSi10Mg alloy in as-built (AB) condition and after three different heat treatments (T5 (4 h at 160 °C), standard T6 (T6B) (1 h at 540 °C followed by 4 h at 160 °C), and rapid T6 (T6R) (10 min at 510 °C followed by 6 h at 160 °C)). In-situ tensile tests were conducted with scanning electron microscopy combined with electron backscattering diffraction. In all samples the crack nucleation was at defects. In AB and T5, the interconnected Si network fostered damage at low strain due to the formation of voids and the fragmentation of the Si phase. T6 heat treatment (T6B and T6R) formed a discrete globular Si morphology with less stress concentration, which delayed the void nucleation and growth in the Al matrix. The analysis empirically confirmed the higher ductility of the T6 microstructure than that of the AB and T5, highlighting the positive effects on the mechanical performance of the more homogeneous distribution of finer Si particles in T6R.
The AlSi10Mg alloy produced by laser-based powder bed fusion (L-PBF) is widely used to produce high-value-added structural parts subjected to cyclic mechanical loads at high temperatures. The paper aims to widen the knowledge of the room- and high-temperature (200 °C) fatigue behavior of the L-PBF AlSi10Mg alloy by analyzing the fully reversed rotating bending test results on mechanically polished specimens. Two heat-treated conditions are analyzed: T5 (direct artificial aging: 4 h at 160 °C) and novel T6R (rapid solution: 10 min at 510 °C, artificial aging: 6 h at 160 °C). The study highlights that (i) the T6R alloy is characterized by higher fatigue strength at room (108 MPa) and high temperatures (92 MPa) than the T5 alloy (92 and 78 MPa, respectively); (ii) thermal exposure at 200 °C up to 17 h does not introduce macroscopical microstructural variation; (iii) fracture surfaces of the room- and high-temperature-tested specimens show comparable crack initiation, mostly from sub-superficial gas and keyhole pores, and failure propagation mechanisms. In conclusion, the L-PBF AlSi10Mg alloy offers good cyclic mechanical performances under various operating conditions, especially for the T6R alloy, and could be considered for structural components operating at temperatures up to 200 °C.
In recent years, the AlSi10Mg alloy produced by laser‐based powder bed fusion (L‐PBF) has gained more attention for increasing the strength‐to‐weight ratio in structural parts subjected to severe operating conditions. Herein, the effects of thermal exposure (0–48 h at 200, 210, and 245 °C) on the metastable microstructure of the L‐PBF AlSi10Mg alloy and the high‐temperature (200 °C) tensile properties post‐overaging (41 h at 210 °C) of the heat‐treated alloy is investigated. In particular, two specific heat treatment conditions, currently neglected in the literature, are analyzed: i) T5 heat treatment (direct artificial aging: 4 h at 160 °C), and ii) the innovative T6R heat treatment (rapid solution: 10 min at 510 °C, and artificial aging: 6 h at 160 °C). The T5 shows a lower decrease in mechanical properties after thermal exposure and during the high‐temperature tensile test than the T6R. This behavior is related to the higher efficiency of the submicrometric cellular structure in hindering the dislocation motion. In addition, the T5 has good tensile properties compared to high‐temperature Al–Si–Mg‐ and Al–Si–Cu–Mg‐casting alloys, representing an attractive option in future industrial applications characterized by operating temperatures up to 200 °C.
Additive processes like Laser Beam Powder Bed Fusion (PBF-LB) result in a distinctive microstructure characterized by metastability, supersaturation, and finesse. Post-process heat treatments modify microstructural features and tune mechanical behavior. However, the exposition at high temperatures can induce changes in the microstructure. Therefore, the present work focuses on the analyses of the tensile response at room and high (200 °C) temperature of the A357 (AlSi7Mg0.6) alloy processed by PBF-LB and subjected to tailored T5 (direct aging) and T6R (rapid solution treatment, quenching, and aging) treatments. Along with the effect of microstructural features in the as-built T5 and T6R alloy, the role of typical process-related defects is also considered. In this view, the structural integrity of the alloy is evaluated by a deep analysis of the work-hardening behavior, and quality indexes have been compared. Results show that T5 increases tensile strength at room temperature without compromising ductility. T6R homogenizes the microstructure and enhances the structural integrity by reducing the detrimental effect of defects, resulting in the best trade-off between strength and ductility. At 200 °C, tensile properties are comparable, but if resilience and toughness moduli are considered, as-built and T5 alloys show the best overall mechanical performance.
In the last decades, several anodizing processes for Mg alloys have been proposed to achieve a good wear and corrosion resistance combination. In particular, Electro-Chemical Oxidation (ECO) showed an improved dense and compact anodized layer compared to other anodizing processes carried out above the dielectric breakdown voltage, such as Plasma Electrolytic Oxidation (PEO). However, the influence of the ECO treatment on the tribological behavior and cyclic mechanical performance of Mg alloys has not been investigated yet. This paper reports on the influence of ECO on dry sliding behavior (vs. 100Cr6 bearing steel (block-on-ring contact geometry)) and rotating bending fatigue performance of the rare earth (RE)-containing Mg alloy EV31A-T6, comparing it with both untreated EV31A-T6 and PEO-treated EV31A-T6, used as benchmarks. The ECO-treated alloy showed improved tribological behavior (critical load for coating failure one order of magnitude higher and coefficient of friction 40% lower than for PEO) and fatigue strength (no decrease for ECO-treated samples compared to the untreated alloy, while PEO-treated samples induced a 15% decrease) due to the increased compactness and lower defectivity of the anodized layer, induced by the minimization of destructive arc discharges during coating growth. In addition, the ECO treatment significantly improved wear resistance compared to the untreated alloy, avoiding, at the same time, the decrease in fatigue strength, which typically occurs after PEO. Therefore, the ECO process can be applied to improve wear resistance without decreasing the fatigue strength of high-performance components.