One of the most important limitations of the atomic force microscopy (AFM) is scanning speed, whose high values are required for contemporary high-resolution, long-range diagnostic applications. The measurement bandwidth of an AFM depends on several factors, but usually results from the time constant of the oscillating cantilever, which is correlated with its resonance frequency and quality factor. We propose a method to overcome this problem by performing the surface measurements when the cantilever is vibrating in higher eigenmodes. In this paper we demonstrate the application of active piezoresistive cantilevers operating in this mode. The active piezoresistive cantilever comprises a piezoresistive deflection sensor, a deflection actuator and a nanotip. It is a complete micro-electro-mechanical system, ensuring the highest reliability of cantilever vibration control and detection. Higher eigenmode operations are usually difficult to implement as they usually result in lower deflection and lower sensitivity of the probe vibration deflection. Here we present an experimental modification of the structure of an active piezoresistive cantilever using focused ion beam machining that mitigates both weaknesses. This has enabled the cantilever to scan the surface at a scanning rate of 10 lines s⁻¹ with a maximum speed of 500 μm s⁻¹ and a data acquisition rate of 10 kS s⁻¹, when the probe is vibrating at 380 kHz in the second eigenmode. We also describe a traceable calibration routine (based on analysis of the response of the piezoresistive detector, the output of the HeNe interferometer and precise control of the deflection actuator), together with the cantilever modification process and the development of the measurement setup. We show measurement results of dedicated calibration samples and silicon carbide crystal lattice references.

This paper presents the possibilities of applying atomic force microscopy (AFM) techniques to the study of the wear of prosthetic biomaterials. In the conducted research, a zirconium oxide sphere was used as a test piece for mashing, which was moved over the surface of selected biomaterials: polyether ether ketone (PEEK) and dental gold alloy (Degulor M). The process was carried out with constant load force in an artificial saliva environment (Mucinox). An atomic force microscope with an active piezoresistive lever was used to measure wear at the nanoscale. The advantage of the proposed technology is the high resolution of observation (less than 0.5 nm) in the three-dimensional (3D) measurements in a working area of 50 × 50 × 10 µm. The results of nano wear measurements in two measurement setups are presented: zirconia sphere (Degulor M and zirconia sphere) and PEEK were examined. The wear analysis was carried out using appropriate software. Achieved results present a tendency coincident with the macroscopic parameters of materials.

In this paper, we report a novel application of atomic force microscopy (AFM) for measurement of wear of prosthetic materials. In contrast to previously employed methods, we introduce AFM-based wear induction. In this way, we utilize AFM as both measurement technique and the mean for surface wear. We describe the methodology along with the metrological advantages of the approach regarding the supreme resolution of volume measurement (down to 1 μm³). We investigate wear between prosthetic gold alloy (Degulor M) and FGP polymeric material from Bredent in nanoscale. For that purpose, we modify active piezoresistive cantilever, replacing the original tip with Degulor M microsphere. We elaborate on the process of modification and present how the mass volume and topology of the tip is controlled throughout the process. Wear process was performed in reciprocal motion over the length of 5 μm in 35,000 repetitions to mimic the actual conditions occurring in human mouth cavity. We present how this method, by focusing on a small area of investigated materials, leads to shortening the overall time of wear measurements from tong term observations down to several minutes. AFM-measured data present consistent relation between wear energy and wear volume. Exemplary results seem to confirm durability of the FGP-Degulor M mechanical contact and occurring strengthening of the mechanical contact with roughening of the polymeric surface.

Wear of dental materials during mastication critically affects prosthetic durability, yet precise nanoscale quantification remains challenging. Here we present a novel method employing a microelectromechanical system (MEMS) active piezoresistive cantilever modified with a fragment of human dental enamel to simulate occlusal contact. Controlled nanoscratching under defined normal forces and cycles enabled quantitative evaluation of wear between enamel and prosthetic substrates such as gold and chromium alloys. Results demonstrate accurate measurement of material volume loss and correlation with nanomechanical energy input, with wear figures as low as 36 μm/N/cycle for enamelgold alloy pairs. This approach preserves authentic tooth–material interfaces and offers high-resolution mapping of early wear stages. The method holds promise for advancing nanoscale tribological assessment of dental biomaterials, potentially informing the development of more durable prosthetic solutions.