As a viscohyperelastic material, filled rubber is widely used as a damping element in mechanical engineering and vehicle engineering. Academic and industrial researchers commonly need to evaluate the fatigue life of these rubber components under cyclic load, quickly and efficiently. The currently used method for fatigue life evaluation is based on the S–N curve, which requires very long and costly fatigue tests. In this paper, fatigue-to-failure experiments were conducted using an hourglass rubber specimen; during testing, the surface temperature of the specimen was measured with a thermal imaging camera. Due to the hysteresis loss during cyclic deformation, the temperature of the material was found to first rise and then level off to a steady state temperature, and then it rose sharply again as failure approached. The S–N curve in the traditional sense was experimentally determined using the maximum principal strain as the fatigue parameter, and a relationship between the steady state temperature increase and the maximum principal strain was then established. Consequently, the steady state temperature increase was connected with the fatigue life. A couple of thousand cycles was sufficient for the temperature to reach its steady state value during fatigue testing, which was less than one tenth of the fatigue life, so the fatigue life of the rubber component could be efficiently assessed by the steady state temperature increase.
The mechanical behaviour of carbon-black (CB)-filled rubber is temperature-dependent. It is assumed that temperature affects the fatigue life of rubber products by changing the tear energy of the material. The static tearing behaviour and fatigue crack propagation behavior of CB-filled rubber at different temperatures were investigated in this study. The critical tear energy of the material was measured through static tear fracture tests at different temperatures; it is shown that the critical tear energy decreases exponentially with increasing temperature. A fatigue crack growth test of a constrained precracked planar tension specimen was conducted at room temperature; the measurements verify that the fatigue crack growth follows a Paris–Erdogan power law. Considering the temperature dependence of the critical tear energy, the temperature dependent fatigue crack growth kinetics of CB-filled rubber was established, and the fatigue life of the material at high temperatures was predicted based on the kinetics. The predictions are in good agreement with experimental measurements.
The mechanical behavior of asphalt mixture under high stresses presents nonlinear viscoelasticity and permanent deformation. In this paper, a nonlinear fractional viscoelastic plastic (NFVEP) creep model for asphalt mixture is proposed based on the Nishihara model, with a Koeller spring-pot replacing the Newton dashpot. The NFVEP model considers the instantaneous elasticity, viscoelasticity with damage and time-hardening viscoplasticity with damage concurrently, and the viscoelastic response is modeled by fractional derivative viscoelasticity. To verify the model, uniaxial compressive creep tests under various stresses ranging from 0.4 MPa to 0.8 MPa were carried out at room temperature. The NFVEP model predictions are in good agreement with the experiments. The comparison with the modified Nishihara model and the Burgers model reveals the advantages of the NFVEP model. The results show that the NFVEP model, with the same set of parameters, can not only describe the primary and steady-state creep stages of asphalt mixture under low stress levels but also the whole creep process, including the tertiary creep stage, of asphalt mixture under high stress levels.
In the tire industry, the Payne effect and hysteresis loss of carbon-black (CB) filled rubber vulcanizates are the most concerning issues. CB filled rubber vulcanizates are susceptible to thermo-oxidative aging in the applications. In this paper, the effects of thermo-oxidative aging are investigated from experimental and theoretical aspects. The specimens are subjected to thermo-oxidative aging at 80, 100 and 120 °C for various periods of time ranging from 1 to 6 days and then the dynamic mechanical tests are conducted. The results show that both the storage modulus and the loss modulus increase with increasing aging time. The hysteresis loss of the material shows an increasing tendency with the increase of dynamic strain amplitude, aging time and aging temperature. The Kraus model is used to describe the Payne effect and a viscoelastic model consisting of dynamic strain amplitude and loss modulus is used to calculate the energy dissipation.
In order to quantitatively describe the time-varying mechanical properties of asphalt mixture during creep process, a nonlinear viscoelastoplastic creep model was proposed, by using variable-order fractional calculus. The differential order of the variable-order fractional element of the model is no longer constant, but a variable that changes with time, which reflects the changes of the mechanical properties of the material during the creep process. Whereas the tertiary creep phase is modeled by the viscoplastic element with time-varying viscosity, which is attributed to damage evolution. The uniaxial creep compression tests of AC-13C asphalt mixture under different stress levels (0.7 MPa, 0.9 MPa, 1.1 MPa, 1.3 MPa, 1.5 MPa, 1.7 MPa) were carried out with MTS-809 testing machine at 25 °C, and the test results were analyzed by the model using Levenberg–Marquardt optimization algorithm. It is shown that creep damage occurs when the applied stress exceeds a certain critical value, and the damage incubation time depends on the applied stress level. The higher stress decreases the damage incubation time. The model is in good agreement with the experimental results, and is applicable to describe the entire creep process, which consists of primary, steady and tertiary stages. Moreover, the variation of the model parameter can describe the change of viscoelastic properties of the material during the creep process. The differential order of the variable-order fractional element is constant during the primary creep stage, indicating that the creep behavior of the asphalt mixture is linear viscoelastic in small strain range. For the same stress level, the fractional order of the steady creep stage is greater than that of the primary creep stage, and it increases with the increasing stress level, which shows that the viscous behavior in the steady creep is more remarkable than that in the primary creep, and the higher the stress level, the more prominent the viscous performance exhibits.
The performance of a viscoelastic damper is governed by the mechanical properties of the viscoelastic material, which are sensitive to prestrain. Among viscoelastic materials, carbon black (CB)-filled rubber vulcanizate is commonly used in structural applications. In this paper, the prestrain-dependent Payne effect and hysteresis loss of CB-filled rubber vulcanizates are investigated through experimental and theoretical analysis. Based on the experimental results, the classic quantitative models proposed by Kraus, Huber–Vilgis, and Maier–Göritz are used to describe the Payne effect. The results show that the Maier–Göritz model is most suitable to describe the Payne effect, especially for the loss modulus. After calculating the area of the hysteresis loops, hysteresis loss curves at various dynamic strain amplitudes are parallel to each other. Through application of the time–strain superposition principle, the hysteresis loss at any arbitrary prestrain can be predicted. Thus, the aim of this paper is to provide guidance for researchers in choosing an accurate model for future investigations of the prestrain-dependent Payne effect. An accelerated characterization method is useful for the prediction of the hysteresis loss of rubber products using small amounts of experimental data, which can provide manufacturers with more attractive and lower cost opportunities for testing the mechanical properties of rubber products.