Aluminum and A356 alloy foam castings are produced using a melt-foaming method. Prior to foaming, the melt is modified with nano-sized particles (SiC, TiN, or Al₂O₃). The nano-sized particles are mixed with micro-sized Al particles, which are ultrasonically treated and hot-extruded. Thus, the so-called “modifying nano-composition” is obtained. The resulting compositions are introduced into the melt of the Al foam at the following mass concentrations of nanoparticles: SiC: 0.038 wt. %; TiN: 0.045 wt. %; and Al₂O₃: 0.046 wt. %. For the A356 foam, we use the following concentrations: SiC: 0.039 wt. %; TiN: 0.052 wt. %; and Al₂O₃: 0.086 wt. %. The macrostructure of the foam castings is investigated by CT scanning and 3D analysis. The pore size distributions and accumulative fraction dependencies are determined for all samples. The microstructure of the foam castings is investigated by SEM-EDS analysis. The results confirmed the presence of individual nano-sized particles, as well as clusters of particles in foam walls. The conducted compression tests show a significant increase in the plateau stress (up to 237%) of the modified aluminum foam castings compared to non-modified castings. However, a similar effect of the nano-compositions on A356 alloy foam castings is not observed. The obtained results show that the above-indicated concentrations of nanoparticles can positively influence the mechanical properties of aluminum foam castings. The novelty of the current study is two-fold: (1) such low concentrations of added nanoparticles have never been used before to alter Al foam’s properties, and (2) an original method of introducing the nanoparticles into the melt is applied in the form of nano-compositions.

The process of hardening a hypereutectic aluminium-silicon alloy AlSi18 in unmodified, modified and nano-modified state has been studied. Two types of modifiers have been used - a standard modifier P, introduced into the melt by means of the ligature CuP 0,4wt.%, and a nanomodifier (nanodiamonds - ND) 0,1wt.%. The influence of the various types of modifiers on the process of crystallization, as well as on the size of the primary Si crystals in the structure of the alloy and their distribution in it has also been discussed.

Two types of A356 alloy castings in initial and modified with nanoparticles condition produced by gravitational casting were studied. Samples, as-cut from the castings, were subjected to light optical microscopy (LM), thermal analyses, Electron Backscattered Diffraction (EBSD) and Scanning Transmission Electron Microscopy (STEM) analyses. Results, obtained by EBSD, confirmed that there is grain refinement in samples from castings with added nanoparticles compared to the initial ones. STEM analysis shows agglomerates of nanoparticles in examined foils. Nanoparticles’ position in the microstructure confirms the hypothesis that they act as nucleating sites during the alloy solidification, which is the reason for observed fine-grained microstructure.

The technological process of the centrifugal casting of short and long castings is examined during development. The values of the technological parameters at applying heat-resistant coating on the working surface of metal molds were established. With a high-speed camera, the temperature of the free surface during the pouring of the melts was measured. Research experiments were conducted. A mathematical model of the centrifugal casting process with a horizontal axis was created.

Composite wires obtained from aluminum shell, micron-sized aluminum powder and nanosized TiN, SiC and Al2O3 powders were fabricated by a two-stage process. The stages included ultrasonic treatment and hot extrusion. TEM and SEM observations were performed to investigate the wires’ microstructure. Individual nanopowder particles as well as particle agglomerations were observed by two microscopic methods, as well as nanoparticles distribution and localization in the matrix. It was found that the observed nanoparticles and clusters were located in the volume of micron-sized Al particles and along the grain boundaries of the matrix. The provided EDX analysis confirms the presence of nanoparticles in the aluminum matrix. From the obtained results, it can be concluded that the two-stage fabrication process of nanocomposite wires leads to better wetting of the nanopowders from the aluminum melt. Nanocomposites obtained by mixing and extruding TiN, SiC and Al2O3 nanopowders and Al micropowder can be used as modifiers of aluminum alloys, as the nanoparticles will contribute to grain refinement and will participate as additional crystallization centers.