Increasing demand of lightweight structures with exceptional properties elicits materials processing and manufacturing technologies to tailor blanks in order to achieve or enhance those prerequisite properties. Friction stir processing (FSP) is a solid-state material processing technique, which was derived from friction stir welding (FSW). Initially, FSP was invented to refine the microstructure in way that superplasticity in a material can be achieved. Afterward, FSP has gained much more attraction as a solid-state grain refinement technique to improve the mechanical, tribological, and corrosion properties in a wide range of low strength non-ferrous and high strength steels. FSP is well capable to produce material with microstructure in range of few micron to nanoscale, depending on the processing conditions. Researchers have investigated FSP at different process parameters such as tool rotation and travel speeds, number of passes, and additional cooling in order to evaluate the impact on the resulting properties for different alloys. Recently, FSP has begun to modify the microstructure and properties in hard alloys and superalloys with some modifications in FSP tooling system. Furthermore, FSP has shown great potential to repair or modify the weld or coating structure by microstructure refinement. Therefore, the present review will discuss the state-of-the-art of FSP under the main categories of microstructure evolution, and effect of process parameters. This review also provides a comprehensive summary of research progress on FSP in different materials i.e. aluminum, magnesium, copper, and steels with the contents much emphasized on the microstructure refinement in terms of average grain size and resulting properties like hardness, tensile, wear, and corrosion. Finally, FSP as a new post-processing approach in weld or coating structure has been discussed.

In the present investigation, dissimilar materials such as electrolytic tough pitch copper, and aluminum 6061-T651 were welded by friction stir welding technology. Effects of tool tilt angle on the mechanical and metallurgical properties were studied experimentally for dissimilar material systems. In the present study, the tool tilt angle was varied from 0° to 4° with an interval of 1°, while the other parameters such as rotational speed, welding speed, tool pin offset, and workpiece material position were kept constant. Macrostructure analysis, tensile test, macro hardness measurement, scanning electron microscopy, and energy dispersive x-ray spectrographic tests were performed to evaluate the weld properties of dissimilar copper–aluminum joints. The results revealed that a defect free dissimilar copper–aluminum friction stir welding was achieved by tilt angles 2°, 3°, and 4°. The maximum tensile strength was reported to be 117 MPa and the macro hardness was reported to be 181 VH (in the nugget zone) at a tilt angle of 4°. The macro hardness was increased as the tilt angle increases from 0° to 4°. In addition to this, the thermo-mechanically affected zone (at the copper side) was found to be the weakest zone for a dissimilar copper–aluminum friction stir welding system.

Poor tribological properties restrict structural applications of aluminum alloys, surface composites of aluminum alloys have gained more attention in material processing. Addition of solid lubricant reinforcement particles along with abrasive ceramics contributes to the enhancement of tribological performance of surface composites. In the present study, solid-state technique, friction stir processing (FSP) was used to develop mono (B₄C) and hybrid (B₄C+MoS₂) surface composites in AA6061-T651 aluminum alloy. The hybrid surface composites were produced by varying an amount of MoS₂. Multipass FSP with different direction strategy was adopted for achieving uniform distribution of reinforcement powders in the aluminum matrix. Microstructure analysis showed a uniform dispersal of reinforcement particles without any clustering or agglomeration in the processing zone. Microhardness and wear performance of mono and hybrid composites improved in comparison to the base metal. Mono surface composite exhibited the highest hardness while hybrid surface composite (75%B₄C+25%MoS₂) achieved the highest wear resistance. This was attributed to the solid lubricant nature of MoS₂. Furthermore, dissolution of strengthening precipitate condition during multipass FSP without reinforcement particles resulted in the reduction of hardness and wear resistance.

The metal matrix composites combine the metallic properties of a tough and ductile matrix with properties of reinforcement particles, simultaneously develop the functional properties by proper selection of reinforcements for projected applications. However, hard ceramics reinforcements decrease toughness and ductility of soft matrix and restrict their wide applications. The surface metal matrix composites (SMMCs) preserve the matrix properties with added advanced surface properties by reinforcing particles only in the surface layer. The hybrid surface metal matrix composites (HSMMCs) with more than one reinforcement gained attention in material processing due to their noble tribological behavior and surface properties, which cannot be attained in mono composites. Conventional liquid-phase processing techniques to fabricate hybrid surface composites result in the formation of undesirable brittle compounds, detrimental to desirable properties of composites. Friction stir processing (FSP), a solid-state processing technique, has been used by many investigators using different reinforcements to fabricate mono as well as hybrid surface composites. Friction stir processed (FSPed) hybrid surface composites have not been extensively reviewed. The current review provides a comprehensive understanding of the latest developments of FSP in hybrid surface composites manufacturing. This paper review different reinforcement strategies in the fabrication of FSPed hybrid surface composites and also the effects of single-pass, multipass, and change in pass direction on microstructure and resultant properties. Finally, future directions and challenges to FSPed hybrid surface composites are summarized. This review article containing important information on hybrid surface composites fabrication by FSP will be useful to academicians and investigators in the field.