The aim of this work was to correlate the overall carbon content in NbC-Ni, NbC-Ni-VC and NbC-Ni-Mo starting powders with the resulting microstructure, hardness, and fracture toughness of Ni-bonded NbC cermets. A series of NbC-Ni, NbC-Ni-VC and NbC-Ni-Mo cermets with different carbon content were prepared by conventional liquid phase sintering for 1 h at 1420 °C in vacuum. Microstructural analysis of the fully densified cermets was performed by electron probe microanalysis (EPMA) to assess the effect of carbon and VC or Mo additions on the NbC grain growth and morphology. A decreased carbon content in the starting powder mixtures resulted in increased dissolution of Nb, V, and Mo in the Ni binder and a decreased C/Nb ratio in the NbC based carbide phase. The Vickers hardness (HV₃₀) and Palmqvist indentation toughness were found to decrease significantly with an increasing carbon content in the Mo-free cermets, whereas an antagonistic correlation between hardness and toughness was obtained as a function of the Mo-content in Mo-modified NbC cermets. To obtain optimized mechanical properties, methods to control the total carbon content of NbC-Ni mixtures were proposed and the prepared cermets were investigated in detail.

In this article, we focus on utilising electrical impedance spectroscopy (EIS) for the assessment of global and contact impedances in roller bearings. Our primary objective is to establish a quantitative prediction of lubricant film thickness in elasto-hydrodynamic lubrication (EHL) and investigate the impedance transition from ohmic to capacitive behaviour as the system shifts from boundary lubrication to EHL. To achieve this, we conduct measurements of electrical impedance, bearing and oil temperature, and frictional torque in a cylindrical roller thrust bearing (CRTB) subjected to pure axial loading across various rotational speeds and supply oil temperatures. The measured impedance data is analysed and translated into a quantitative measure of lubricant film thickness within the contacts using the impedance-based and capacitance-based methods. For EHL, we observe that the measured capacitance of the EHL contact deviates from the theoretical value based on a Hertzian contact shape by a factor ranging from 3 to 11, depending on rotational speed, load, and temperature. The translation of complex impedance values to film thickness, employing the impedance and capacitance method, is then compared with the analytically estimated film thickness using the Moes correlation, corrected for inlet shear heating effects. This comparison demonstrates a robust agreement within 2% for EHL film thickness measurement. Monitoring the bearing resistance and capacitance via EIS across rotational speeds clearly shows the transition from boundary to mixed lubrication as well as the transition from mixed lubrication to EHL. Finally, we have observed that monitoring the electrical impedance appears to have the potential to perform the run-in of bearings in a controlled way.

In this research work, unfilled and mono-filled polytetrafluoroethylene (PTFE) materials were developed and characterised by physical, thermal, viscoelastic, mechanical, and wear analysis. The applied fillers were graphene, alumina (Al₂O₃), boehmite alumina (BA80), and hydrotalcite (MG70) in 0.25/1/4/8 and 16 wt % filler content. All samples were produced by room temperature pressing–free sintering method. All of the fillers were blended with PTFE by intensive dry mechanical stirring; the efficiency of the blending was analysed by Energy-dispersive X-ray spectroscopy (EDS) method. Compared to neat PTFE, graphene in 4/8/16 wt % improved the thermal conductivity by ~29%/~84%/~157%, respectively. All fillers increased the storage, shear and tensile modulus and decreased the ductility. PTFE with 4 wt % Al₂O₃ content reached the lowest wear rate; the reduction was more than two orders of magnitude compared to the neat PTFE.

Additive manufacturing (AM) of polymeric materials offers many benefits, from rapid prototyping to the production of end-use material parts. Powder bed fusion (PBF), more specifically selective laser sintering (SLS), is a very promising AM technology. However, up until now, most SLS research has been directed toward polyamide powders. In addition, only basic models have been put forward that are less directed to the identification of the most suited operating conditions in a sustainable production context. In the present combined experimental and theoretical study, the impacts of several SLS processing parameters (e.g., laser power, part bed temperature, and layer thickness) are investigated for a thermoplastic elastomer polyester by means of colorimetric, morphological, physical, and mechanical analysis of the printed parts. It is shown that an optimal SLS processing window exists in which the printed polyester material presents a higher density and better mechanical properties as well as a low yellowing index, specifically upon using a laser power of 17–20 W. It is further highlighted that the current models are not accurate enough at predicting the laser power at which thermal degradation occurs. Updated and more fundamental equations are therefore proposed, and guidelines are formulated to better assess the laser power for degradation and the maximal temperature achieved during sintering. This is performed by employing the reflection and absorbance of the laser light and taking into account the particle size distribution of the powder material.