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Muhammad Faizan Ul Haq
Lecturer, University of Lahore (UOL), Islamabad, Pakistan

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Journal article
Published: 01 April 2021 in Proceedings of the Institution of Civil Engineers - Transport
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This research work aims to enhance the performance of asphalt binder using multi-walled carbon nanotubes (MWCNTs) incorporating the wet mixing technique. Five asphaltic binder compositions were prepared with varying amount of MWCNTs additions ranging from 0.0 to 1.50 (%w/w). The performance was evaluated by investigating the basic viscoelastic properties, rheological characteristics and moisture susceptibility. Viscoelastic properties were assessed through penetration, softening point, ductility and dynamic shear rheometer (DSR) tests. Rolling bottle test (RBT) was used for moisture sensitivity analysis.. Fourier Transmission Infrared Spectroscopy (FTIR) was used to check various solvent's chemical reactivity with asphalt binder, whereas Scanning Electron Microscopy (SEM) was used to observe the level of MWCNTs dispersion in the mixture. Samples were also checked for storage stability. Furthermore, safety analysis was carried out for the selection of the appropriate carrier solvent. It was observed that the adapted hypothesis leads to an improvement in permanent deformation and stripping resistance of binders. Addition of MWCNTs by 1.5 (%w/w) of asphalt binder reduced penetration grade by 14.4% with an increase of 10.2% and 40% in softening point and ductility respectively. Furthermore, considerable improvements in phase angle and dynamic shear modulus were observed accompanied by 50% reduction in stripping after 24 hours.

ACS Style

Waqas Anwar; Naveed Ahmad; Anwar Khitab; Muhammad Faizan; Seemab Tayyab; Maria Saeed; Muhammad Imran. Performance augmentation of asphalt binder with multi-walled carbon nanotubes. Proceedings of the Institution of Civil Engineers - Transport 2021, 174, 130 -141.

AMA Style

Waqas Anwar, Naveed Ahmad, Anwar Khitab, Muhammad Faizan, Seemab Tayyab, Maria Saeed, Muhammad Imran. Performance augmentation of asphalt binder with multi-walled carbon nanotubes. Proceedings of the Institution of Civil Engineers - Transport. 2021; 174 (2):130-141.

Chicago/Turabian Style

Waqas Anwar; Naveed Ahmad; Anwar Khitab; Muhammad Faizan; Seemab Tayyab; Maria Saeed; Muhammad Imran. 2021. "Performance augmentation of asphalt binder with multi-walled carbon nanotubes." Proceedings of the Institution of Civil Engineers - Transport 174, no. 2: 130-141.

Review
Published: 01 June 2020 in Emerging Materials Research
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In recent years, various nanomaterials have been used in many scientific and engineering fields. Owing to their small size and large surface area, nano-modifiers result in improved substrate characteristics in comparison to their macro and micro-sized counterparts. Nanomaterials possess incredible features, which make them suitable as additives in asphalt mixtures. This study describes the importance of nanomaterials with emphasis on the use of Carbon nanotubes as asphalt binder modifier. Different methods for synthesis of CNTs such as arc discharge, laser ablation and chemical vapor deposition (CVD) are explained, and different types of techniques used for CNTs dispersion in bitumen are elaborated. The results of conventional testing techniques such as penetration grade, softening point, ductility and viscosity to characterize the mechanical performance of CNTs modified asphalt binder are also summarized in this work. Effects of CNTs modifications on the rheological properties of asphalt binder have also been described. A systematic review of experimental studies on asphalt binder modification using CNTs was carried out. Addition of CNTs improves the stiffness of asphalt binder thereby increasing its resistance against rutting. Different parameters/variables such as binder type, mixing technique, mixer type, CNTs properties and mixing time play key roles in modification of bitumen with CNTs by significantly effecting the performance of the resulting asphalt binder.

ACS Style

Muhammad Faizan Ul Haq; Naveed Ahmad; Muhammad Jamal; Waqas Anwar; Anwar Khitab; Sabahat Hussan. Carbon Nanotubes and Their Use for Asphalt Binder Modification: A Review. Emerging Materials Research 2020, 9, 1 -16.

AMA Style

Muhammad Faizan Ul Haq, Naveed Ahmad, Muhammad Jamal, Waqas Anwar, Anwar Khitab, Sabahat Hussan. Carbon Nanotubes and Their Use for Asphalt Binder Modification: A Review. Emerging Materials Research. 2020; 9 (2):1-16.

Chicago/Turabian Style

Muhammad Faizan Ul Haq; Naveed Ahmad; Muhammad Jamal; Waqas Anwar; Anwar Khitab; Sabahat Hussan. 2020. "Carbon Nanotubes and Their Use for Asphalt Binder Modification: A Review." Emerging Materials Research 9, no. 2: 1-16.

Article
Published: 17 February 2019 in Applied Sciences
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With the increase in the demand for bitumen, it has become essential for pavement engineers to ensure that construction of sustainable pavements occurs. For a complete analysis of the pavement, both its structural and functional performances are considered. In this study, a novel material (i.e., Graphene Nano-Platelets (GNPs)) has been used to enhance both of the types of pavements’ performances. Two percentages of GNPs (i.e., 2% and 4% by the weight of the binder) were used for the modification of asphalt binder in order to achieve the desired Performance Grade. GNPs were homogeneously dispersed in the asphalt binder, which was validated by Scanning Electron Microscope (SEM) images and a Hot Storage Stability Test. To analyze the structural performance of the GNPs-doped asphalt, its rheology, resistance to permanent deformation, resistance to moisture damage, and bitumen-aggregate adhesive bond strength were studied. For the analysis of the functional performance, the skid resistance and polishing effect were studied using a British Pendulum Skid Resistance Tester. The results showed that GNPs improved not only the rutting resistance of the pavement but also its durability. The high surface area of GNPs increases the pavement’s bonding strength and makes the asphalt binder stiffer. GNPs also provide nano-texture to the pavement, which enhances its skid resistance. Thus, we can recommend GNPs as an all-around modifier that could improve not only the structural performance but also the functional performance of asphalt pavements.

ACS Style

Murryam Hafeez; Naveed Ahmad; Mumtaz Ahmed Kamal; Javaria Rafi; Muhammad Faizan Ul Haq; Jamal; Syed Bilal Ahmed Zaidi; Muhammad Ali Nasir. Experimental Investigation into the Structural and Functional Performance of Graphene Nano-Platelet (GNP)-Doped Asphalt. Applied Sciences 2019, 9, 686 .

AMA Style

Murryam Hafeez, Naveed Ahmad, Mumtaz Ahmed Kamal, Javaria Rafi, Muhammad Faizan Ul Haq, Jamal, Syed Bilal Ahmed Zaidi, Muhammad Ali Nasir. Experimental Investigation into the Structural and Functional Performance of Graphene Nano-Platelet (GNP)-Doped Asphalt. Applied Sciences. 2019; 9 (4):686.

Chicago/Turabian Style

Murryam Hafeez; Naveed Ahmad; Mumtaz Ahmed Kamal; Javaria Rafi; Muhammad Faizan Ul Haq; Jamal; Syed Bilal Ahmed Zaidi; Muhammad Ali Nasir. 2019. "Experimental Investigation into the Structural and Functional Performance of Graphene Nano-Platelet (GNP)-Doped Asphalt." Applied Sciences 9, no. 4: 686.

Journal article
Published: 17 December 2018 in Applied Sciences
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Conventional binders cannot meet the current performance requirements of asphaltic pavements due to increase in traffic volumes and loads. Nanomaterials, due to their exceptional mechanical properties, are gaining popularity as bitumen modifiers to enhance the performance properties of the asphaltic concrete. Carbon Nanotubes (CNTs) are one of the most widely used nanomaterials because of their strength properties, light weight, small size, and large surface area. CNT addition results in improved substrate characteristics as compared to other modifiers. Due to high length to diameter ratio, dispersion of CNTs in bitumen is a complex phenomenon. In this study, dispersion of CNTs in bitumen was carried out using both dry and wet mixing techniques, the latter was selected on the basis of homogeneity of the resultant asphalt mixture. Scanning Electron Microscopy (SEM) was used to check the dispersion of CNTs in binder while Fourier Transform Infrared Spectroscopy (FTIR) was carried out to ensure the removal of solvent used for wet mixing. Conventional bitumen tests (penetration, softening point, and ductility), dynamic shear rheometer tests, rolling bottle tests, and bitumen bond strength tests were employed to check the improvement in the rheological and adhesion properties of bitumen while wheel tracker test was used to check the improvement in resistance against permanent deformation of asphalt mixtures after addition of CNTs. Results show that CNTs improved the higher temperature performance and permanent deformation resistance in both binder and mixtures. Improvement in bitumen–aggregate adhesion properties and moisture resistance was also observed.

ACS Style

Muhammad Faizan Ul Haq; Naveed Ahmad; Muhammad Ali Nasir; Jamal; Murryam Hafeez; Javaria Rafi; Syed Bilal Ahmed Zaidi; Waqas Haroon. Carbon Nanotubes (CNTs) in Asphalt Binder: Homogeneous Dispersion and Performance Enhancement. Applied Sciences 2018, 8, 2651 .

AMA Style

Muhammad Faizan Ul Haq, Naveed Ahmad, Muhammad Ali Nasir, Jamal, Murryam Hafeez, Javaria Rafi, Syed Bilal Ahmed Zaidi, Waqas Haroon. Carbon Nanotubes (CNTs) in Asphalt Binder: Homogeneous Dispersion and Performance Enhancement. Applied Sciences. 2018; 8 (12):2651.

Chicago/Turabian Style

Muhammad Faizan Ul Haq; Naveed Ahmad; Muhammad Ali Nasir; Jamal; Murryam Hafeez; Javaria Rafi; Syed Bilal Ahmed Zaidi; Waqas Haroon. 2018. "Carbon Nanotubes (CNTs) in Asphalt Binder: Homogeneous Dispersion and Performance Enhancement." Applied Sciences 8, no. 12: 2651.

Journal article
Published: 10 July 2018 in Applied Sciences
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Applications of nanotechnology in the pavement industry have increased rapidly during the last decade in order to enhance a pavement’s sustainability and durability. Conventional asphalt binder generally does not provide sufficient resistance against rutting at high temperatures. Carbon black nano-particles (CBNPs, produced by perennial mountain trees’ carbonization) were mixed into the performance grade (PG) 58 asphalt binder in this study. Conventional asphalt binder tests (penetration, ductility and softening point), frequency sweep, performance grading, and bitumen bond strength tests were conducted to study the enhancement in the properties of asphalt binder. Dynamic modulus and wheel tracking tests were also performed to investigate the effect of CBNPs on asphalt mixture properties. Experimental results demonstrated that preferred dosage of CBNPs in asphalt is 10% by weight of the bitumen. Results of scanning electron microscopy (SEM) and storage stability tests validated homogenous and stable dispersion of CBNPs in the asphalt binder. Asphalt mixtures became stiffer and resistant to rutting at high temperatures by addition of CBNPs in asphalt binder. Significant improvement in bitumen aggregate bond strength was also observed by incorporating CBNPs. It is concluded that CBNPs can be used to effectively enhance the high-temperature performance and consequently the sustainability of flexible pavements.

ACS Style

Javaria Rafi; Mumtaz Ahmed Kamal; Naveed Ahmad; Murryam Hafeez; Muhammad Faizan Ul Haq; Syeda Aamara Asif; Faisal Shabbir; Syed Bilal Ahmed Zaidi. Performance Evaluation of Carbon Black Nano-Particle Reinforced Asphalt Mixture. Applied Sciences 2018, 8, 1114 .

AMA Style

Javaria Rafi, Mumtaz Ahmed Kamal, Naveed Ahmad, Murryam Hafeez, Muhammad Faizan Ul Haq, Syeda Aamara Asif, Faisal Shabbir, Syed Bilal Ahmed Zaidi. Performance Evaluation of Carbon Black Nano-Particle Reinforced Asphalt Mixture. Applied Sciences. 2018; 8 (7):1114.

Chicago/Turabian Style

Javaria Rafi; Mumtaz Ahmed Kamal; Naveed Ahmad; Murryam Hafeez; Muhammad Faizan Ul Haq; Syeda Aamara Asif; Faisal Shabbir; Syed Bilal Ahmed Zaidi. 2018. "Performance Evaluation of Carbon Black Nano-Particle Reinforced Asphalt Mixture." Applied Sciences 8, no. 7: 1114.