This study was conducted to test possibilities of application of 3D printed dental models (DMs) in terms of their accuracy and physical properties. In this work, stone models of mandibles were cast from alginate impressions of 10 patients and scanned in order to obtain 3D printed acrylic replicas. The diagnostic value was tested as matching of model scans on three levels: peak of cusps, occlusal surface, and all teeth surfaces. The mechanical properties of acrylic and stone samples, specifically the impact strength, shore D hardness, and flexural and compressive strength were investigated according to ISO standards. The matching of models’ surfaces was the highest on the level of peaks of cusps (average lack of deviations, 0.21 mm) and the lowest on the level of all teeth surfaces (average lack of deviations, 0.64 mm). Acrylic samples subjected to mechanical testing, as expected, showed higher mechanical properties as compared to the specimens made of dental stone. In the present study we demonstrated that 3D printed acrylic models could be ideal representatives in the case of use as a diagnostic tool and as a part of medical records. The acrylic samples exhibited not only higher mechanical properties, but also showed better accuracy comparing to dental stone.
The fractionation of diatomaceous earth (DE) using sedimentation made it possible to obtain separate unbroken diatom fractions from broken or agglomerated bodies with a range of particle sizes. The produced filler was used to prepare polylactide (PLA)/diatomaceous earth biocomposite samples containing different particle sizes, which were subjected to mechanical testing (tensile strength, flexural strength, impact strength), colloidal testing (contact angle, color change test, SEM/EDS), and thermal testing (TGA, DSC, DMA). Modification of the PLA containing the smallest particle size with diatomaceous earth (Fraction 5) resulted in a higher impact strength compared to both the pure PLA and the PLA/DE composite that contained base diatomaceous earth. Furthermore, the melt flow rate was improved by more than 80 and 60% for the composite modified with fractionated diatomaceous earth (Fraction 4) compared to pure PLA and base diatomaceous earth, respectively. The elasticity of the composite was also improved from 3.3 GPa for pure polylactide to 4.4 GPa for the system containing the smallest diatomaceous earth particles (Fraction 5).
This study investigates the influence of solution treatment temperatures on the microstructure and mechanical properties of LPBF (Laser Powder Bed Fusion)-manufactured Inconel 939 alloy. The primary objectives are to assess the impact of sub-recrystallization (below recrystallization temperature) and recrystallization temperatures during solution treatment on mechanical performance under different conditions. This study validates the hypothesis concerning carbide redistribution and mechanical performance in LPBF-produced Inconel 939 parts through comprehensive analysis, including microstructure studies and tensile tests. The results indicate that higher heat treatment temperatures lead to significant changes in carbide redistribution and mechanical performance. For instance, at room temperature, the specimen with sub-recrystallization solution treatment temperature exhibited superior mechanical properties compared to both the as-built and recrystallization-temperature solution treatment specimens. However, at elevated temperatures (700 °C), a reversal in mechanical anisotropy was observed, with the vertical axis demonstrating higher tensile strength compared to the horizontal axis for all material states. Furthermore, a microstructural analysis revealed distinct changes in grain structure and precipitate distribution, particularly the migration of carbides from grain boundaries to intragranular regions. These findings underscore the importance of precise control over heat treatment parameters to achieve optimal mechanical behavior. This research provides valuable insights into optimizing LPBF processes for the Inconel 939 alloy, highlighting the need for a meticulous control of the solution treatment parameters to ensure mechanical integrity. The findings contribute to a broader understanding of material-specific responses in additive manufacturing, with significant implications for aerospace applications.
Degradation of power engineering steel structures requires constant monitoring of their mechanical properties to estimate remaining service life. Therefore, the current study aimed to develop a methodology that will enable for accurate determination of changes in mechanical properties of 10CrMo9-10 steel after long-term exploitation involving the Small Punch Test (SPT). Firstly, the as-received 10CrMo9-10 steel was annealed at 770 °C for different periods (1.5, 6 and 24 h) to deteriorate its strength to a level similar to its exploited counterpart. Then, mechanical properties were characterized by uniaxial tensile tests and the SPT method using miniaturized discs with a diameter of 8 mm and a thickness of 0.5 mm as recommended by the EN 10371:2021 standard. It allowed to determine a formula correlating the SPT results (i.e., elastic–plastic transition force and maximum force) with the yield and ultimate tensile strength. The βRp0.2 and βRm correlation factors were equal to 0.437 and 0.255, respectively. Finally, the exploited 10CrMo9-10 steel was tested by the SPT method. Based on the SPT results, the values of Rp0.2 = 236 ± 27 MPa and Rm = 459 ± 17 MPa were estimated, which were close to those assessed during the uniaxial tensile tests (Rp0.2 = 218 ± 3 MPa and Rm = 454 ± 4 MPa). It was shown that the application of such a relatively simple method is a promising way for determining the changes in mechanical properties of structural steels after long-term service at elevated temperature.
13 September 2025 in Journal of Materials Research and Technology