Polymer products manufactured by additive processes are today increasingly flooding the market. Given that they have broad application ranging from various consumer products to medicine and automotive industry, the products must satisfy certain mechanical properties. In the past studies of selective laser sintering (SLS) for polymer materials, the processing parameter of energy density has been confirmed which affects the tensile properties. Energy density depends on the laser beam speed, laser power and hatch distance; however, in this paper the existing mathematical model has been expanded by the overlay ratio and tests have been conducted how on the basis of the new mathematical model a product with good tensile properties (tensile strength, tensile strength at break, tensile modulus, tensile strain at break) can be manufactured. However, in parameter selection as well, the layer thickness and the manufacturing strategy also play a role, and they may shorten the time and reduce the cost necessary to manufacture a new product from the initial concept to production. The paper also provides a proposal of processing parameters (laser beam speed, laser power and energy density) depending on the manufacturing strategy and layer thickness.
From the very start of their use until today, processes in Additive Manufacturing (AM) have found a way to grow from prototype production to individual and small-series production. Improvements in machinery, materials and other challenges in AM development have improved product quality, its mechanical properties and dimensional accuracy. Research in the field of dimensional accuracy must be focused on achieving better tolerances. From the beginning of AM, there has been a big issue in assuring dimensional repeatability and reproducibility of a part being printed over the course of several days. In order to examine that, a test plate was designed and built repeatedly with PolyJet technology over the course of several weeks. Measurements of dimensional accuracy and shape deviations of several typical features were carried out using X-ray Computed Tomography. Measurement results were analysed and presented in order to indicate the repeatability and reproducibility of PolyJet AM technology. Results show that PolyJet technology consistently produces parts within ±100 μm, at a 95% confidence interval, under reproducibility conditions of over a 1-month period. Accuracy for measurands (distance) in the x and y axis was significantly better than it was for the z axis which was from 56 to 197 µm, i.e., in the x and y axis, it was from −8 to 76 µm. Shape errors (i.e., cylindricity) were larger than positional or dimensional errors; this can be attributed to relatively large surface roughness and small feature sizes on the test plate that was used.
The automotive industry is one of the biggest consumers of polymer composites. Aside from good mechanical properties, polymer composites have low mass, which positively affects the overall vehicle weight reduction and improves energy efficiency. Although polymer composites are used in various vehicle components, this paper focused on the application in vehicle bumper production. Two different composite plates with hybrid fiber layup were made; the first plate with a combination of glass and carbon fibers and the second with carbon and aramid. For comparison, and as a cheaper variant, a third plate was made only with glass fibers. In the first two plates, epoxy resin was used as the matrix, while in the third plate, polyester resin was used. Polyurethane memory foams of different densities (60, 80, 100 kg/m3) and thicknesses (10, 15, 20 mm) were used as impact force energy absorbers. With the factorial design of experiments, it was found that the thickness of the memory foam was the main influence factor. Without the use of memory foam, the hybrid composite, made of glass and carbon fibers, showed the highest energy absorption, while with the use of foam, the highest energy absorption was achieved with the glass fiber composite. Without the memory foam, the impact force measured on the glass/carbon hybrid composite was 9319.11 ± 93.18 N. Minimum impact force to the amount of 5143.19 ± 237.65 N was measured when the glass fiber composite plate was combined with the memory foam. When using memory foam, the impact force was reduced by 30–48%, depending on the type of composite used.
The aim of this research was to investigate the compressive strength (CS), breaking strength (BS), and compressive modulus (CM) of conventional glass ionomer cement (GIC) modified with TiO2 nano particles, marine-derived hydroxyapatite (md-HAp) microparticles (<45 µm), and a combination of TiO2 NP and md-HAp particles. The materials used in the study were conventional GIC Fuji IX GP Extra (GC Corporation, Tokyo, Japan), TiO2 powder P25 (Degussa, Essen, Germany), and HAp synthesized from cuttlefish bone and ground in a mortar to obtain md-HAp powder. md-HAp was characterized using FTIR and SEM analysis. There were four groups of GIC samples: (i) Fuji IX control group, (ii) powder modified with 3 wt% TiO2, (iii) powder modified with 3 wt% HAp, and (iv) powder modified with 1.5 wt% TiO2 + 1.5 wt% HAp. Measurements were performed in a universal testing machine, and CS, BS, and CM were calculated. Statistical analysis was performed using ANOVA and Tukey’s tests. CS, BS, and CM differed significantly between the Fuji IX control group and all experimental groups while differences between the experimental groups were not statistically significant. The addition of TiO2 NP, md-HAp micro-sized particles, and a combination of TiO2 and md-HAp reduced the CS, BS, and CM of conventional GICs when mixed at the powder/liquid (p/l) ratio recommended by the manufacturer.
(1) Background: Digital technologies are available for denture base fabrication, but there is a lack of scientific data on the mechanical and chemical properties of the materials produced in this way. Therefore, the aim of this study was to investigate the residual monomer content, flexural strength and microhardness of denture base materials as well as correlations between investigated parameters. (2) Methods: Seven denture base materials were used: one conventional heat cured polymethyl methacrylate, one polyamide, three subtractive manufactured materials and two additive manufactured materials. High-performance liquid chromatography was used to determine residual monomer content and the test was carried out in accordance with the specification ISO No. 20795-1:2013. Flexural strength was also determined according to the specification ISO No. 20795-1:2013. The Vickers method was used to investigate microhardness. A one-way ANOVA with a Bonferroni post-hoc test was used for the statistical analysis. The Pearson correlation test was used for the correlation analysis. (3) Results: There was a statistically significant difference between the values of residual monomer content of the different denture base materials (p < 0.05). Anaxdent pink blank showed the highest value of 3.2% mass fraction, while Polident pink CAD-CAM showed the lowest value of 0.05% mass fraction. The difference between the flexural strength values of the different denture base materials was statistically significant (p < 0.05), with values ranging from 62.57 megapascals (MPa) to 103.33 MPa. The difference between the microhardness values for the different denture base materials was statistically significant (p < 0.05), and the values obtained ranged from 10.61 to 22.86 Vickers hardness number (VHN). A correlation was found between some results for the material properties investigated (p < 0.05). (4) Conclusions: The selection of contemporary digital denture base manufacturing techniques may affect residual monomer content, flexural strength and microhardness but is not the only criterion for achieving favourable properties.