Within the scope of the presented work the processing of AISI H11 (1.2343 or X37CrMoV5-1) tool steel powder modified by adding carbon black nanoparticles in varying concentrations by means of Laser Metal Deposition (LMD) is extensively investigated. On the basis of single weld track experiments, multi-layered cuboid-shaped samples made out of pure AISI H11 tool steel powder as well as modified tool steel powder mixtures were manufactured by applying various process parameters. The main scientific aim of the investigations was to achieve a basic understanding of the influence of the added carbon black nanoparticles on the resulting sample properties. For that purpose, the generated specimens were first analyzed with respect to relative density, inner defects, microstructure, Vickers hardness and chemical composition. Subsequently, the mechanical properties of post-heat-treated specimens were investigated, with the focus on the yield strength (Y0.2%), by means of compression tests. We prove that by adding carbon black nanoparticles to the initial AISI H11 powder, the formation of martensitic and bainitic phases, as well as the precipitation of carbides at the grain boundaries, are enhanced. As a result, a significant increase of Vickers hardness and of the compression yield strength by up to 11% can be achieved in comparison to samples made out of the unmodified AISI H11 powder. Furthermore, it can be fundamentally demonstrated that the fabrication of parts with layer-specific variable hardness can be realized by the controlled changing of the powder mixtures used during the layer-by-layer manufacturing approach.
In the field of tool making, Laser Beam Melting of metals has been already used to fabricate injection moulds with complex inner cooling channels made out of the low-carbon maraging tool steel X3NiCoMoTi18-9-5 (1.2709). Furthermore, laser metal deposition (LMD) is an established technology for the repair of worn-out tools and the deposition of wear resistance coatings based on metal matrix composites. However, at the moment, the processing of high-carbon tool steels for the additive manufacturing of complete cold forging tools has only been investigated to a limited extent. Within the scope of the presented research, the processing of the high-carbon cold-work tool steel 60CrMoV18-5 (1.2358) by LMD is analyzed in detail. In this context, geometrically simple cuboidal structures are directly generated on dissimilar substrate plates made out of the hot-work tool steel X37CrMoV5-1(1.2343) via the application of various process parameter combinations. The manufactured cuboidal structures are metallographically prepared and subsequently analyzed with respect to substrate bonding, relative density, defect formation, microstructure, chemical composition, and microhardness. In this context, the influence of the particle size distribution of the used tool steel powder on the LMD process itself and the resulting relative density are extensively researched. For this purpose, high-speed camera measurements of the powder particle stream were conducted in order to determine both the powder particle stream diameter and the lateral powder particle distribution with regard to the distance z from the powder nozzle. Furthermore, the influence of an additional substrate preheating (maximum preheating temperature of 400 °C) on the resulting microstructure and hardness of the additively generated samples is the subject of the presented investigations.
Powder Bed Fusion with Laser Beam of Metals (PBF-LB/M) is one of the fastest growing technology branches. More and more metallic alloys are being qualified, but processing of aluminum wrought alloys without cracks and defects is still challenging. It has already been shown that small parts with low residual porosity can be produced. However, suffering from microscopic hot cracks, the fracture behavior has been rather brittle. In this paper different combinations of temperature gradients and solidification rates are used to achieve specific solidification conditions in order to influence the resulting microstructure, as well as internal stresses. By this approach it could be shown that EN AW-2024, an aluminum-copper wrought alloy, is processable via PBF-LB/M fully dense and crack-free with outstanding material properties, exceeding those reported for commonly manufactured EN AW-2024 after T4 heat treatment.