In recent years, with increasing engineering applications, structural adhesives have played an increasingly important role in joining both metallic and non-metallic components. Polyurethane is frequently used in the adhesive industry due to its morphological structure, versatile material, and excellent matrix material. In addition, by doping polyurethane with single/multi-walled carbon nanotubes and boron nitride nanoplates materials, the mechanical properties of the polyurethane adhesive can be further increased. This study aimed to increase the mechanical properties of PU (thermoset polyurethane), which is frequently used in adhesively bonded joints by addition of MWCNT (multi-walled carbon nanotubes), BNNP (boron nitride nanoplates). For this purpose, nanoparticles synergistic interaction was investigated by adding a mass of 0.25%, 0.35%, and 0.45% MWCNT into PU, which was reinforced by 0.5% BNNP before. Samples mechanical properties were determined by tensile test according to ASTM D638-10 standard, flexure test according to ASTM D790-02 standard, and Shore D test according to ASTM D2240 standard. All sample test results were graphed, and each graph was compared. Also, broken surfaces were analyzed by scanning electron microscopy (SEM) to examine the damage mechanism of nanoparticles.
11 February 2026 in Journal of Adhesion Science and Technology
Artan enerji taleplerin karşılanmasında yenilenebilir enerji türleri açısından popüler olan fotovoltaik teknolojiler üzerine verim artırmaya yönelik çalışmalar yapılmaktadır. Boya duyarlı güneş pilleri yüksek altyapı maliyeti gerektirmeyen yapılar olduğundan verim artırmaya yönelik çalışmalar boya duyarlı güneş hücreleri (DSSC) üzerine yoğunlaşmıştır. DSSC’de ışığa duyarlı boya, TiO2 tabakasına tutundurulmaktadır. Kullanım ömrünü tamamlamış NiTi alaşımı endodontik eğeler, farklı asitler üzerinden çözeltiye alınıp metalik değerlerine ayrıştırılmış ve bu metalik değerlerden olan anataz fazında olduğu tespit edilen TiO2 ‘nin boya duyarlı güneş hücrelerinde kullanımına yönelik çalışmalar yapılmıştır. Çalışma kapsamında atık NiTi eğelerden elde edilen kontamine TiO2 ‘nin yapısı karakterize edilmiş ve N719 boya çözeltisinin yüzeye tutundurularak optik özellikleri araştırılmıştır. Boya duyarlı güneş hücrelerinde kullanılan N719 boya çözeltisi uygulanan geri kazanım anataz TiO2 tatbik edilmiş yüzeyle ile görünür bölge spektrumunda belirgin bir etkinlik göstermediği ortaya konulmuştur.
29 June 2026 in International Journal of Damage Mechanics
This study reports the synthesis of multilayer Ti 3 C 2 T x MXene through selective etching of Ti 3 AlC 2 and its incorporation into Elium ® thermoplastic resin at loadings of 0.25–1.0 wt.%. The resulting nanocomposites were characterized by scanning electron microscopy (SEM), X-ray diffraction, thermogravimetric analysis/differential scanning calorimetry, and mechanical tests, including tensile (ASTM D638), flexural (ASTM D790), and fracture toughness (ASTM D5045) analyses. The 0.75 wt.% MXene composite exhibited the most balanced performance, achieving a tensile strength of 69.45 MPa, a flexural strength of 110 MPa, and a 31% improvement in fracture toughness over neat Elium ® . These enhancements were attributed to uniform nanofiller dispersion and effective interfacial interaction that facilitates stress transfer and crack deflection. SEM fractography revealed a transition from smooth, brittle fracture surfaces in the neat matrix to rough, branched crack paths in the MXene-filled composites, indicating improved energy dissipation. Overall, MXene/Elium ® nanocomposites showed superior strength, toughness, and thermal stability, highlighting their potential as lightweight and recyclable materials for structural applications in automotive, aerospace, and protective sectors.