A deep knowledge of material properties is fundamental to obtain high‐performance medical implants realized with CoCrMo alloy manufactured by selective laser melting (SLM), even more so when considering that heat treatments (HTs) are often necessary to refine the microstructure, eliminate residual stress, and improve mechanical properties. To this aim, herein, SLM CoCrMo alloy samples are produced in six different treatment conditions: as built (AB), four different vacuum HTs, and hot isostatic pressing (HIP). Modifications to microstructure, hardness, tensile behavior, and wear resistance are then investigated. Results reveal that vacuum HTs and HIP have different effects on microstructure and types of defects with respect to the AB condition. Thus, proper selection of the treatment is mandatory to improve specific mechanical properties, such as strength, ductility, hardness, or tribological response. In this context, it is confirmed that the choice of an appropriate HT allows SLM CoCrMo to reach the target mechanical properties set by international standards for applications in the medical field, such as dentistry or orthopedics.
The European steel industry produces about 70 million tons/year of steel by the electric arc furnace (EAF). The slag consists of about 15% by weight of the produced steel, thus from the perspective of the circular economy, it has a high potential as a co-product. This research aims to assess an innovative reuse of EAF slag as filler in different polymer matrixes: thermoplastic (polypropylene), thermosetting (epoxy resin), elastomeric (nitrile butadiene rubber), and recycled end of life rubber tire. A comparison between neat polymer and polymer filled with a certain amount of EAF slag has been carried out by tensile (or flexural), compression, and hardness tests. Experimental results show that slag as a filler increases the composites’ hardness and elastic modulus at the expense of toughness. For a safe reuse of the slag, the leaching of hazardous elements must comply with current legislation. It was found that, although the used EAF slag releases small amounts of Cr, Mo, and V, incorporating it into a polymer matrix reduces the leaching. The EAF slag particles distribution has been observed by scanning electron microscopy (SEM) images. The obtained results show good technical feasibility of this innovative slag application so that it could pave the way to a new industrial symbiosis between dissimilar sectors, bringing economic and environmental benefits.
19 November 2021 in Advanced Engineering Materials
Additive manufacturing (AM) can be particularly advantageous to manufacture components designed to meet challenging structural requirements. Selective laser melting (SLM) microstructure is different than that obtained by traditional manufacturing process; in particular, mechanical and microstructural features achieved herein are influenced by the entire thermal history, including the manufacturing process and the heat treatment (HT) with relevant role of the slow cooling rate adopted. In fact, both the process and the HTs can significantly modify the microstructure and related mechanical and tribological properties. To better understand how mechanical response can be tuned to meet different requirements, in this article the effects of four different vacuum HTs on microstructures, mechanical properties, and wear behavior of Inconel 625 produced with SLM are deeply investigated. In general, the results confirm that HT can significantly change the microstructure and mechanical or tribological properties of Inconel 625. Among the examined HT, solution + aging and direct aging improve the strength of the alloy, whereas annealing leads to recrystallization, reducing strength in favor of ductility. Stress relieving does not significantly change the microstructure and mechanical properties. Considering tribological behavior, only direct aging HT leads to a remarkable improvement, with a reduction in friction coefficient and wear rate.