In order to improve the utilization rate of kapok fiber, flame-retardant and sound-absorption composites were prepared by the hot pressing method with kapok fiber as the reinforced material, polyε-caprolactone as the matrix material, and magnesium hydroxide as the flame retardant. Then, the effects of hot pressing temperature, hot pressing time, density of composites, mass fraction of kapok fiber, thickness of composites, and air layer thickness on the sound-absorption properties of composites were analyzed, with the average sound absorption coefficient as the index. Under the optimal process parameters, the maximum sound absorption coefficient reached 0.830, the average sound absorption coefficient was 0.520, and the sound-absorption band was wide. Thus, the composites belonged to high-efficiency sound-absorbing material. The flame-retardant effect of magnesium hydroxide on the composites was investigated, and the limiting oxygen index could reach 31.5%. Finally, multifunctional composites based on kapok fiber with flame retardant properties, and sound-absorption properties were obtained.
To broaden the application fields of waste hemp stalks, the macromolecular, supramolecular, and morphological structures of waste hemp stalks were analyzed, and the relationship between these properties and the sound absorption properties of the hemp stalks was explored. Then, waste hemp stalk/polycaprolactone sound-absorbing composite materials were prepared by the hot pressing method. The influence of hemp stalk length and mass fraction, and the density and thickness of the composite materials on the sound absorption properties of composites prepared with the hot pressing temperature set to 140 °C, the pressure set to 8 MPa, and the pressing time set to 30 min was investigated. The results showed that, when the sound energy acts on the hemp stalk, the force between the chain segments, the unique hollow structure, and the large specific surface, act together to attenuate the sound energy and convert it into heat and mechanical energy in the process of propagation, to produce a good sound absorption effect. When the hemp stalk length and mass fraction were set to 6 mm and 50%, respectively, and the density and thickness of the material were set to 0.30 g/cm3 and 1.5 cm, respectively, the average sound absorption coefficient of the waste hemp stalk/polycaprolactone sound-absorbing composite material was 0.44, the noise reduction coefficient was 0.42, the maximum sound absorption coefficient was 1.00, and the sound-absorbing band was wide. The study provided an experimental and theoretical basis for the development of waste hemp stalk/polycaprolactone sound-absorbing composite materials, and provided a new idea for the recycling of the waste hemp stalk.
17 October 2018 in ACS Sustainable Chemistry & Engineering
Conventionally laminated spacer composites are extensively applied in many fields owing to their light weight. However, their impact resistance, interlaminar strength, and integrity are poor. In order to overcome these flaws, the zigzag-shaped 3D woven spacer composites were rationally designed. The zigzag-shaped 3D woven spacer fabrics with the basalt fiber filaments tows 400 tex (metric count of yarn) used as warp and weft yarns were fabricated on a common loom with low-cost processing. The zigzag-shaped 3D woven spacer composites were obtained using the VARTM (vacuum-assisted resin transfer molding) process. The three-point bending deformation and effects of damage in zigzag-shaped 3D woven spacer composites were studied both in experiment and using the finite element method (FEM). The bending properties of zigzag-shaped 3D woven spacer composites with different direction, different numbers of weaving cycle, and different heights were tested in experiments. In FEM simulation, the geometrical model was established to analyze the deformation and damage based on the 3D woven composite structure. Compared with data obtained from the experiments and FEM simulation, the results show good agreement and also prove the validity of the model. Based on the FEM results, the deformation, damage, and propagation of stress obtained from the model are very helpful in analyzing the failure mechanism of zigzag-shaped 3D woven composites. Furthermore, the results can significantly guide the fabrication process of real composite materials.
1 January 2020 in Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy