Hammada scoparia (Pomel) is a powerful plant with important biological properties. In this study, we report on the green synthesis of silver-doped nickel and copper nanoparticles (NPs) in the presence of H. scoparia leaf extract using a self-propagating sol–gel autocombustion process. The synthesized NiO, CuO, Ag-NiO, and Ag-CuO NPs were characterized with Fourier transform infrared spectroscopy (FTIR) and X-ray diffraction (XRD). Afterward, they were tested for their antimicrobial activity as well as their potential to remove dyes from aqueous solutions using adsorption processes for malachite green (MG) and photocatalytic degradation for methylene blue (MB). Our results showed that the mass of the adsorbent had a significant effect on the adsorption rate, which increased to reach a maximum value of 98%. The Ag-CuO NP showed the best final conversion of MB (97.95%) compared to NiO, CuO, and Ag-NiO. In addition, we noted that the NPs doped with silver had the best performance in the removal of dyes. These results indicated that the photocatalytic performance was significantly improved after the addition of silver. Moreover, the antimicrobial activity showed that the studied NPs had moderate activity against the tested bacteria and a weak activity or were ineffective against Candida albicans. Therefore, the green synthesis of NPs from H. scoparia leaf extract is considered a sustainable alternative to removing dyes from aqueous solutions. However, further investigation should be performed on the other dyes to understand the overall effectiveness of these NPs.

In the present work, the extraction and the variation of total phenolic and the flavonoid content of the Halimium halimifolium plant (the leaves and the stems) harvested from Morocco have been studied. It explores extracting the essential oil of this plant and analyzing its chemical composition by the gas chromatography-mass spectrometry (GC/MS). Interesting results have been obtained, in particular, the presence of 26 compounds where the major one is (+)-2-Bornanone (38.26) followed by Eucalyptol (27.74). This essential oil proves great antioxidant capacities which is measured with the total antioxidant activity (TAC) and the organic chemical compound 2,2-diphenyl-1-picrylhydrazyl (DPPH) assays. On the other hand, using solvents with different polarities (the hexane, the dichloromethane, the ethyl acetate, the ethanol, and the water), the quantifying of the total phenolic and the flavonoid content for different crude extracts of the Halimium halimifolium was done. The results show simultaneous increasing in the total phenolic content of the crude extract and the solvent polarity.