In this paper, we analyze the possibilities of the protection of tools for wood machining with PVD (Physical Vapor Deposition) hard coatings. The nanolayered TiN/AlTiN coating, nanocomposite TiAlSiN coatings, and single layer TiN coating were analyzed in order to use them for protection of tools for wood machining. Both nanostructured coatings were deposited in an industrial magnetron sputtering system on the cutting blades made of sintered carbide WC-Co, while TiN single layer coating was deposited by evaporation using thermionic arc. In the case of TiN/AlTiN nanolayer coatings the thickness of the individual TiN and AlTiN layer was in the 5–10 nm range, depending on the substrate vertical position. The microstructure and chemical composition of coatings were studied by scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDS) method. Additionally, in the case of the TiN/AlTiN coating, which was characterized by the best durability characteristics, the transmission electron microscope (TEM) and X-ray photoelectron spectroscopy (XPS) methods were applied. The coatings adhesion to the substrate was analyzed by scratch test method combined with optical microscopy. Nano-hardness and durability tests were performed with uncoated and coated blades using chipboard. The best results durability characteristics were observed for TiN/AlTiN nanolayered coating. Performance tests of knives protected with TiN and TiAlSiN hard coatings did not show significantly better results compared to uncoated ones.
The influence of different types of cemented carbide blades and thickness of TiAlN/a-C:N and TiN/AlTiN protective coatings used in the wood industry on cutting performance has been studied. Three types of WC-Co cemented carbide blades with different cobalt content were used in the study. The thicknesses of both types of coatings were ~2 and ~5 µm. The structure, chemical and phase composition were studied using transmission and scanning electron microscopy (TEM, SEM), X-ray dispersion spectroscopy (EDX) and X-ray diffraction (XRD), respectively. The adhesion was evaluated by scratch test. Nanohardness and durability tests of uncoated and coated blades were performed. We found that the blades covered with 5 µm TiN/AlTiN coatings exhibited the best durability characteristic. The cutting distances were within the range ~6700-~7080 depending on the substrates in comparison with pure substrates (~4300–~4900) and 2 µm TiN/AlTiN coatings (~5400–~6600). The presence of a thin and soft outer a-C:N layer aggravates the nanohardness and durability of the coated blades.
The scientific goal of this paper is to study and explain the relationship between the microstructure of a ceramic–intermetallic composite fabricated by consolidating a mixture of Al2O3 and NiAl-Al2O3 using the PPS technique and its basic mechanical properties. Six series of composites were manufactured. The obtained samples differed in the sintering temperature and content of compo-powder. The base powders, compo-powder, and composites were investigated using SEM equipped with an EDS and XRD. Hardness tests and KIC measurements were applied to estimate the mechanical properties of the fabricated composites. The wear resistance was evaluated using a “ball-on-disc” method. The results demonstrate that the density of the obtained composites increases with the increased temperature of the sintering. The content of NiAl + 20 wt.% Al2O3 did not have a determining effect on the hardness of the manufactured composites. The highest hardness, contacting 20.9 ± 0.8 GPa, was found for the composite series sintered at 1300 °C and 2.5 vol.% of compo-powder. The highest KIC value from all the studied series equaled 8.13 ± 0.55 MPa·m0.5 and was also achieved for the series manufactured at 1300 °C (2.5 vol.% of compo-powder). The average friction coefficient during the ball-friction test with the Si3N4 ceramic counter-sample was between 0.8 and 0.95.
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