The adhesion enhancement of graphene oxide (GO) and reduced graphene oxide (rGO) layer in the underlying polyethersulfone (PES) microfiltration membrane is a crucial step towards developing a high-performance membrane for water purification applications. In the present study, we modified the surface of a PES microfiltration membrane with plasma treatment (PT) carried out at different times (2, 10, and 20 min). We studied the effect of PT on the adhesion, stability, and performance of the synthesized GO/rGO-PES membranes. The membranes’ surface morphology and chemistry were characterized using atomic force microscopy, field emission scanning electron microscopy, and Fourier transform infrared spectroscopy. The membrane performance was evaluated by conducting a diffusion test for potassium chloride (KCl) ions through the synthesized membranes. The results revealed that the 2 min PT enhanced the adhesion and stability of the deposited GO/rGO layer when compared to the other plasma-treated membranes. This was associated with an increase in the KCl ion rejection from ~27% to 57%. Surface morphology analysis at a high magnification was performed for the synthesized membranes before and after the diffusion test. Although the membrane’s rejection was improved, the analysis revealed that the GO layers suffered from micro/nano cracks, which negatively affected the membrane’s overall performance. The use of the rGO layer, however, helped in minimizing the GO cracks and enhanced the KCl ion rejection to approximately 94%. Upon increasing the number of rGO deposition cycles from three to five, the performance of the developed rGO-PES membrane was further improved, as confirmed by the increase in its ion rejection to ~99%.

To understand and quantify casing wear during drilling operations, an experimental setup with real drill pipe joints (DPJ) and casings was designed and used to carry out wear tests, simulating various operating conditions and environments. P110 steel casing samples were tested under dry and wet conditions. Actual field oil- and water-based fluids were utilized to lubricate the contact area at two different side loads (1000 N and 1400 N) and DPJ speeds (115 and 207 rpm). The results show that for the same testing conditions, the casing wear volume and wear factor under water-based lubrication were more than twice those obtained under oil-based fluid testing. As expected, the wear volume and wear factor were highest under dry conditions. Moreover, it was noticed that, as the normal load was increased at a constant rotational speed (rpm), the wear factor increased. On the other hand, raising the rotational speed at the same applied load reduced the casing wear factor, due to the observed absence of adhesive wear and possible localized softening effects at higher speeds. SEM analyses of the worn areas showed that under dry conditions, the main wear mechanisms were abrasion and delamination. However, both adhesive wear and abrasive wear mechanisms were observed under oil-based lubrication. The energy dispersive spectroscopy (EDS) analysis of the worn surface revealed that at higher loads and speeds, a heavy transfer of particles from the oil-based lubricant took place. On the other hand, some contaminants of the water-based lubricant were observed on the worn surfaces.

This work aims to explore the effect of side load and rotational speed on the tribological behavior of a novel ceramic–epoxy composite in Kevlar matrix casing lining that is in contact with a rotating drillpipe tool joint (DP-TJ) coated with the same composite. Three rotational speeds (65, 115, and 154 rpm) and three side loads (500, 700, and 1000 N) were considered under water-based mud (WBM) lubrication. Wear depths, volumes, and specific casing wear rates (K) were determined for each combination of speed and load. The wear depth and K were found to increase with an increasing applied side load. However, the specific casing wear rate at the rotational speed of 115 rpm was found to be the lowest among the three speeds. This is mainly due to a probable lubrication regime change from boundary lubrication at 65 rpm to hydrodynamic lubrication with a thick lubricant film at 115 rpm. The digital microscope images were used to determine the wear mechanism, showing that at low speeds, the main mechanism was abrasive wear, but the increase in the speed brought about more adhesive wear. In contrast, the change in the side load does not affect the wear mechanism of the casing. Scanning electron microscopy and energy-dispersive spectroscopy (EDS) were used to analyze the surface and composition of the novel material before and after the wear tests.

This work aims to explore the impact of side loads, drill-pipe tool-joint (DP-TJ) speed (rpm), and mud type on the austenitic stainless steel SM2535-110 casing wear characteristics. Actual field drill pipe tool joints, casings, and drilling muds are used in this study. The results of the study show that under both types of lubrication, the wear volume increased with radial load and DP-TJ speed. SM2535-110 casing specimens tested under oil-based mud (OBM) lubrication had higher casing wear volumes than those obtained under water-based mud (WBM) lubrication. This unexpected behavior is mainly due to the increase in the surface hardness of the casing specimens tested under WBM. The results also show that the specific wear rate or wear factor (K) (which is defined as the volume loss per unit load per unit distance sliding) values of specimens tested under WBM are in general two to four times higher than those obtained under OBM. While K values under WBM increase with both the side load and rpm, those under OBM show a sharp decrease with rpm. This behavior under OBM is due to this lubricant’s higher viscosity and the change of lubrication regime from thin film to thick film lubrication at higher rpm. Scanning electron microscopy (SEM) and the digital microscopic imaging (DMI) of SM235-110 casing specimens show that an aggressive combination of adhesive, abrasive, and plastic deformation was observed under WBM, while the dominant wear mechanism under OBM is abrasive wear.

This work aims to explore the impact of side loads, drill-pipe tool-joint (DP-TJ) speed (RPM), and mud type on the austenitic stainless steel SM2535-110 casing wear characteristics. Actual field drill pipe tool joints, casings, and drilling muds are used in this study. The results of the study show that under both types of lubrication, the wear volume increased with radial load and DP-TJ speed. SM2535-110 casing specimens tested under oil-based mud (OBM) lubrication had higher casing wear volumes than those obtained under water-based mud (WBM) lubrication. This unexpected behavior is mainly due to the increase in the surface hardness of the casing specimens tested under WBM. The results also show that the specific wear factor (K) values of specimens tested under WBM are in general 2 to 4 times higher than those obtained under OBM. While K values under WBM increase with both the side load and RPM, those under OBM show a sharp decrease with RPM. This behavior under OBM is due to this lubricant’s higher viscosity and the change of lubrication regime from thin film to thick film lubrication at higher RPM. Scanning electron microscopy (SEM) and the digital microscopic imaging (DMI) of SM235-110 casing specimens show that an aggressive combination of adhesive, abrasive, and plastic deformation was observed under WBM, while the dominant wear mechanism under OBM is abrasive wear.