This paper presents a novel approach for edge detection and concatenation. It applies the proposed method on a set of optical microscopy images of aluminium alloy Al 99.5% (ENAW1050A) samples with different grain size values. The performance of the proposed approach is evaluated based on the intercept method and compared with the manual grain size determination method. Edge detection filters have proven inefficient in grain boundaries’ detection of the presented microscopy images. To some extent only the Canny edge-detection filter was able to compute grain boundaries of lower-resolution images adequately, while the presented method proved to be superior, especially in high-resolution images. The proposed method has proven its applicability, and it implies higher automatisation and lower processing times compared to manual optical microscopy image processing.

Besides a wide application in corrosion protection, wear resistance increase, providing thermal properties and power conversion, oxide coatings have found an alternative application in welding technology as catalysts of the tungsten inert gas (TIG) welding process. In this paper, the novel approach of fabricating a coating containing nanoparticles based on nanosized SiO₂ and TiO₂ and their mixtures was applied to the austenitic stainless-steel base metal. It was found that coatings increased depths of penetration, enabling a consumable-free welding. Using this method, the use of several critical and near-critical raw materials (e.g., Si and Cr), as well as the relatively expensive Ni can be completely avoided. The most effective coating in terms of weld penetration consisted of a mixture of nanoparticles, rather than unary oxide coatings based on nanoparticles. A model for liquid weld metal flow is proposed based on the metallographic examination of recrystallized grains and microhardnesses measured near the weld metal, supporting the reversed Marangoni convection theory.

The aim of this study was to study the influence of TiO₂ coating for its efficacy during the activated-tungsten inert gas (TIG) welding and to suppress the use of consumables that are rich in critical raw materials. Post-welding penetration depth, particle size distribution, microstructure, and microhardness of welded samples were assessed. Based on these results, it was found that there is no direct correlation between the weld metal surface area and the coating. The particle size in the coating, although, seemed to have played an important role, e.g., nanoparticles resulted in an increased penetration depth and depth/width (D/W) ratio as opposed to the submicron-sized particles. The most optimal welding condition resulted when a mixture of submicron-sized and nanometric-sized particles were used. It was demonstrated by the Zeta analyser results that the micron particles rub the nanoparticles due to mechanical friction resulting in smaller oxide particle formation in the coating. Finally, the presence of Marangoni convection in TIG and reversed Marangoni convection in the activated TIG (A-TIG) process were proven by means of the microstructure analysis and measurement, which were found to be positively correlated.

Austenitic stainless steels represent a significant aerospace material, being used for various castings, structural components, landing gear components, afterburners, exhaust components, engine parts, and fuel tanks. The most common joining process is tungsten inert gas (TIG) welding, which possesses many advantages such as suitability to weld a wide range of ferrous and non-ferrous metals and alloys, providing high quality welds with good mechanical properties. Its major disadvantage is low productivity due to low penetration and welding speed. This can be overcome by introducing an activating flux before welding. The activating flux reverses the material flow of the weld pool, significantly increasing penetration. Therefore, shielding gas consumption is reduced and welding without a consumable is enabled. However, the consumable in conventional TIG also enables the conditioning of the mechanical properties of welds. In this study, Si and Ti metallic oxide nanoparticles were used to increase the weld penetration depth, while bend testing, tensile, and impact toughness were determined to evaluate the mechanical properties of welds. Furthermore, optical emission spectroscopy, light, and scanning electron microscope were used to determine the chemical compositions and microstructures of the welds. Chemical compositions and weld mechanical properties were similar in all specimens. The highest tensile and impact properties were obtained with the specimen welded with the flux containing 20% TiO₂ and 80% SiO₂ nanoparticles. Although lower than those of the base metal, they were well within the nominal base metal mechanical properties.

Bobbin tool friction stir welding (BTFSW) is a variant of the FSW process which uses the special two-shoulder tool that forms the top and bottom of a weld surface. As such, a significant simplification of the welding setup is achieved. One of the dominant parameters of the BTFSW process is the interference between the tool shoulder pinch gap and the weld metal thickness. In this research, the influence of interference of the square pin tool with convex shoulders on process temperature, microstructure, tensile, impact, and bend performance were studied, and appropriate correlations were devised. The base metal was an aluminum–magnesium alloy in which the interference varied in the range of 0.1 to 0.5 mm. Wormhole defects and irregularities were found in all specimens except in the specimen welded with 0.4 mm interference. An optimal interference of 0.4 mm resulted in the best mechanical properties, which, in terms of tensile strength and reduction of area, were similar to the base metal. Furthermore, the impact strength was significantly higher, which was attributed to the grain refinement effect in the nugget zone.

Hardfacing is a welding-related technique aimed at depositing a harder and tougher layer onto a softer, less wear-resistant substrate or base metal. This process enhances the abrasion resistance of the component, increasing its durability under working conditions. A key feature of hardfacing is dilution, which refers to the mixing of the hardfacing layer and the base metal. In this study, shielded metal arc welding (SMAW) was employed to hardface structural steel using chromium carbide vanadium consumables, with results compared to AISI D2 cold-work tool steel. Four different SMAW parameters were tested, and the abrasive test was conducted against SiC discs. Wear rate, represented by the wear loss rate, was correlated to microstructure, scanning electron microscopy, energy-dispersive X-ray spectroscopy, hardness, microhardness, and surface roughness. The results showed that key SMAW parameters, such as welding speed and current, significantly influence wear resistance. Specifically, slower welding speeds and higher currents, which result in greater heat input, led to the increased wear resistance of the deposited layer through the mechanism of the inoculation of larger and harder carbides.