Prestrained at 5% and 15% duplex stainless steel UNS S32750 specimens have been subjected to electropulsing treatments with current density of 100 A/mm2 and 200 A/mm2 and 100 and 500 pulses for each current density value. Corrosion tests, X-ray diffraction, microhardness and residual stresses were collected before and after the electropulsing treatments. Tensile tests were performed after the electropulsing treatments in order to compare the mechanical response to reference tensile tests performed before pulsing treatments. Increase in fracture strain was observed after pulsing treatment in comparison to the reference tensile tests. A decrease in microhardness was also observed after electropulsing treatments for both degrees of prestrain. Electropulsing treatment almost eliminates the work-hardened state in the 5% prestrained specimens while partially recovered the 15% prestrained material increasing both uniform and fracture strain. Bulk temperature of the samples remained the same for all treatments duration. The effect are to be addressed to a combined effect of increase in atomic flux due to the electrical current and local joule heating in correspondence of crystal defects. Electropulsing treatment applied to metallic alloys is a promising technique to reduce the work hardening state without the need of annealing treatments in a dedicated furnace.
Duplex and Super Duplex Stainless Steels are very prone to secondary phases formation related to ferrite decomposition at high temperatures. In the present paper the results on secondary phase precipitation in a 2510 Duplex Stainless Steel, heat-treated in the temperature range 850–1050 °C for 3–30 min are presented. The precipitation starts at grain boundaries with a consistent ferrite transformation for very short times. The noses of the Time–Temperature–Precipitation (TTP) curves are at 1000 °C for σ-phase and at 900 °C for χ-phase, respectively. The precipitation sequence involves a partial transformation of χ into σ, as previously evidenced in 2205 and 2507 grades. Furthermore, the experimental data were compared to the results of Thermo-Calc calculations. Understanding and ability to predict phase stability in 2510 duplex stainless steel is a key factor to design optimal welding processes that avoid any secondary phase precipitation in the weld bead as well as in the heat-affected zone.
During the production of forged metal components, the sequence of heat treatments that are carried out, as well as hot working, remarkably influences mechanical properties of the product, in particular impact toughness. It is possible to tailor impact toughness by varying tempering temperature and soaking time after hardening treatment, widening the application range of structural steels. In this work, we consider the effects of a second tempering treatment on the microstructural properties and impact toughness of a structural steel EN 10025-6 S690 (DIN StE690, W. n: 1.8931). The steel was first forged and quenched in water after austenitization at 890 °C for 4 h. After quenching different tempering treatments were performed, at 590 °C in single or multiple steps. The effect of these treatments was evaluated both in microstructural terms, by means of optical microscopy, scanning and transmission electron microscopy and X-ray diffraction, and in terms of impact toughness. The mechanical behavior was correlated with the microstructure and a remarkable increase in impact toughness was found after the second tempering treatment due to carbide shape change.
Duplex stainless steels (DSSs), a particular category of stainless steels, are employed in all kinds of industrial applications where excellent corrosion resistance and high strength are necessary. These good properties are provided by their biphasic microstructure, consisting of ferrite and austenite in almost equal volume fractions of phases. In the present work, Nd: YAG pulsed laser dissimilar welding of UNS S32750 super duplex stainless steel (SDSS) with 316L austenitic stainless steel (ASS), with different heat inputs, was investigated. The results showed that the fusion zone microstructure observed consisted of a ferrite matrix with grain boundary austenite (GBA), Widmanstätten austenite (WA) and intragranular austenite (IA), with the same proportion of ferrite and austenite phases. Changes in the heat input (between 45, 90 and 120 J/mm) did not significantly affect the ferrite/austenite phase balance and the microhardness in the fusion zone.
15 June 2024 in Journal of Materials Research and Technology
The cladding process reduces manufacturing costs by depositing super austenitic stainless steel onto low-carbon steel. Arc welding techniques, especially gas tungsten arc welding (GTAW), are commonly used for this purpose. This study evaluates the influence of heat input on cladding performance. Macroscopic analysis showed good fusion of the weld beads to the base metal with no defects. Higher heat input resulted in a lower dilution rate due to increased reinforcement. A microstructural analysis of the heat-affected zones revealed similar characteristics, with martensite formation attributed to cooling conditions. Increased microhardness was observed at the interface between the cladding and base metal, corroborating the microstructural findings. Additionally, a significant enhancement in corrosion resistance was noted in the deposited layers. This research contributes to optimizing cladding processes, ensuring better material performance in industrial applications.