The present work aims to understand the effect of chemical treatment on the physical and mechanical characteristics of the natural fibers, namely, areca frond fibers, banana, and flax fibers. Chemical reagents viz. sodium bicarbonate, potassium permanganate, and chromium sulfate were used for surface modifications. Tensile strength of the fibers was determined for analyzing the influence of treatments. Scanning electron microscopy was adopted to visualize the surface morphology. Fourier transform infrared spectroscopy was performed on the fiber specimen to interpret functional group modifications. The research results indicated a decrease in fiber diameter with increase in density of fibers post treatments. For areca frond and flax fibers, chromium sulfate treatment was the most effective while that for banana fibers sodium bicarbonate based treatment turned out to be most effective over the others. Scanning electron microscopy images confirmed clear visibility of fiber inner cell structure, protruding secondary fibrils for treated fibers, reagent coating on the fiber surface was also observed in the case of chromium sulfate-treated samples. Fourier transform infrared spectroscopy analysis showed distinct bands indicating functional group modifications corresponding to cellulose, hemicellulose, and lignin.

The effect of resin modification through the incorporation of the biomass waste in the form of seashell powder on the mechanical properties of basalt fiber–reinforced epoxy/seashell composites is examined through experimental investigations. The resin modification is done through the addition of seashell powder in 5, 10, 15, and 20 wt.%. The modified resin is then reinforced with basalt fiber mat and the required laminate is obtained through compression molding technique. The specimens required for various mechanical tests, such as flexural, tensile, inter laminar shear (ILSS), and the impact strengths, are cut from the laminate as per the standard ASTM dimensions. The mechanical test results indicate that through the addition of the seashell filler additional toughening mechanisms are introduced which improves the strength of the composite laminate. The improvement in the flexural modulus value for all the laminates made from modified resin indicates the ability of the laminate to deflect the applied load effectively and efficiently. The optimum wt.% addition of seashell filler into the resin is found to be 5% for flexural, ILSS, and impact strength while for tensile strength it was observed to be 10%. The addition of higher wt.% loading of seashell filler into the resin has rendered the resin too thick and viscous with minimum flowability. Thus, there is a reduced wettability of the modified resin with the basalt fibers due to which the strength of the laminates reduces. The SEM analysis indicates widespread delamination for higher wt.% addition of the seashell filler into the resin.

The global push for sustainable materials has intensified the research on natural fiber-reinforced composites. This study investigates the potential of sugarcane bagasse fibers, combined with a bio-based epoxy matrix, as a sustainable alternative for high-performance composites. A comprehensive approach was adopted, including wear testing, thermal and structural characterization, and machine learning predictive modeling. Ethylene dichloride-treated fibers exhibited the lowest wear rate (0.245 mg/m) and the highest thermal stability (T20% = 260 °C, char yield = 1.3 mg), highlighting the role of optimized surface modifications. XRD (X-ray diffraction) analysis revealed that pre-treated fibers achieved the highest crystallinity index of 62%, underscoring the importance of structural alignment in fiber-matrix bonding. Machine learning insights using a Random Forest model identified fiber treatment as the most significant parameter influencing wear performance, with accurate predictions validated through experimental results. This work demonstrates the transformative potential of sugarcane bagasse fibers in sustainable polymer composites, offering a pathway for environmentally friendly, lightweight, and durable material solutions. These findings integrate experimental rigor with computational insights, paving the way for advancements in natural fiber-based composite technologies.