This research investigates the effects of steel (ST) and synthetic (SYN) fibers on the workability and mechanical properties of HPFRC. It also analyzes their influence on the material’s microstructural characteristics. ST fibers improve tensile strength, fracture toughness, and post-cracking performance owing to their rigidity, mechanical interlocking, and robust adhesion with the matrix. SYN fibers, conversely, mitigate shrinkage-induced micro-cracking, augment ductility, and enhance concrete performance under dynamic stress while exerting negative effects on workability. Hybrid fiber systems, which include ST and SYN fibers, offer synergistic advantages by enhancing fracture management at various scales and augmenting ductility and energy absorption capability. Scanning electron microscopy (SEM) has been crucial in investigating fiber–matrix interactions, elucidating the effects of ST and SYN fibers on hydration, crack-bridging mechanisms, and interfacial bonding. ST fibers establish thick interfacial zones that facilitate effective stress transfer, whereas SYN fibers reduce micro-crack formation and enhance long-term durability. Nonetheless, research deficiencies persist, encompassing optimal hybrid fiber configurations, the enduring performance of fiber-reinforced concrete (FRC), and sustainable fiber substitutes. Future investigations should examine multi-scale reinforcing techniques, intelligent fibers for structural health assessment, and sustainable fiber alternatives. The standardization of testing methodologies and cost–benefit analyses is essential to promote industrial deployment. This review offers a thorough synthesis of the existing knowledge, emphasizing advancements and potential to enhance HPFRC for high-performance and sustainable construction applications. The findings facilitate the development of new, durable, and resilient fiber-reinforced concrete systems by solving current difficulties.

Integrating class-C and class-F fly ash (FA) as supplementary cementitious materials (SCMs) in concrete offers a promising pathway for sustainable construction practices. This study explores the pivotal role of FA in reducing carbon dioxide (CO₂) emissions and improving concrete’s durability and mechanical properties through a comprehensive life cycle analysis (LCA). By blending FA with cement, significant reductions in CO₂ emissions are achieved, alongside enhancements in the workability, compressive strength, and permeability resistance of the concrete matrix. This research elucidates the pozzolanic reaction between FA and calcium hydroxide (CH) during cement hydration, highlighting its contribution to concrete strength and durability. Through a range of comprehensive analysis techniques, including mechanical testing and environmental impact assessment, this study demonstrates the substantial benefits of prioritizing the utilization of class-C and class-F FA in sustainable construction. The findings underscore the industry’s commitment to environmentally conscious practices, promoting structural integrity and reducing ecological impacts. Overall, this research emphasizes class-C and class-F FA as critical components in achieving sustainable construction goals and advancing towards a more environmentally responsible built environment.

Structural lightweight concrete (SLWC) is crucial for reducing building weight, reducing structural loads, and enhancing energy efficiency through lower thermal conductivity. This study explores the effects of incorporating silica fume (SF), micro-polypropylene (micro-PP), and macro-PP fibers on the workability, thermal properties, and strength of SLWC. SF was added to all mixtures, substituting 10% of the Portland cement (PC), except for the control mixture. Macro-PP fibers were introduced alone or in combination with micro-PP fibers at volumetric ratios of 0.3% and 0.6%. The study evaluated various parameters, including slump, Vebe time, density, water absorption (WA), ultrasonic pulse velocity (UPV), thermal conductivity coefficients (k), compressive strength (CS), and splitting tensile strength (STS) across six different SLWC formulations. The results indicate that while SF negatively impacted the workability of SLWC mortars, it improved CS and STS due to the formation of calcium silicate hydrate (C-S-H) gels from SF’s high pozzolanic activity. Additionally, using micro-PP fibers in combination with macro-PP fibers rather than solely macro-PP fibers enhanced the workability, CS, and STS of the SLWC samples. Although SF had a minor effect on reducing thermal conductivity, the use of macro-PP fibers alone was more effective for improving thermal properties by creating a more porous structure compared to the hybrid use of micro-PP fibers. Moreover, increasing the ratio of micro- and macro-PP fibers from 0.3% to 0.6% resulted in lower CS values but a significant increase in STS values.