Nitrogen is used as an alloying element, substituting the expensive and allergenic element nickel, in austenitic stainless steels to improve their mechanical properties and corrosion resistance. The development of austenitic stainless steel powders with increased nitrogen content for laser additive manufacturing has recently received great interest. To increase nitrogen content in the austenitic steel powders (for example AISI 316L), two measures are taken in this study: (1) melting the steel under a nitrogen atmosphere, and (2) adding manganese to increase the solubility of nitrogen in the steel. The steel melt is then atomized by means of gas atomization (with either nitrogen or argon). The resulting powders are examined and characterized with regard to nitrogen content, particle size distribution, particle shape, microstructure, and flowability. It shows that about 0.2–0.3 mass % nitrogen can be added to the austenitic stainless steel 316L by adding manganese and melting the steel under nitrogen atmosphere. The particles are spherical in shape and very few satellite particles are observed. The steel powders show good flowability and packing density, therefore they can be successfully processed by means of laser powder bed fusion (L-PBF).

Al matrix composites reinforced with 40 vol% Fe_50.1Co_35.1Nb_7.7B_4.3Si_2.8 glassy particles have been produced by powder metallurgy, and their microstructure and mechanical properties have been investigated in detail. Different processing routes (hot pressing and hot extrusion) are used in order to consolidate the composite powders. The homogeneous distribution of the glassy reinforcement in the Al matrix and the decrease of the particle size are obtained through ball milling. This has a positive effect on the hardness and strength of the composites. Mechanical tests show that the hardness of the hot pressed samples increases from 51–155 HV, and the strength rises from 220–630 MPa by extending the milling time from 1–50 h. The use of hot extrusion after hot pressing reduces both the strength and hardness of the composites: however, it enhances the plastic deformation significantly.

Laser additively manufactured duplex stainless steels contain mostly ferrite in the as-built parts due to rapid solidification of the printed layers. To achieve duplex microstructures (ferrite and austenite in roughly equal proportions) and, thus, a good combination of mechanical properties and corrosion resistance, an austenitic stainless steel powder (X2CrNiMo17-12-2) and a super duplex stainless steel powder (X2CrNiMoN25-7-4) were mixed in different proportions and the powder mixtures were processed via PBF-LB/M (Laser Powder Bed Fusion) under various processing conditions by varying the laser power and the laser scanning speed. The optimal process parameters for dense as-built parts were determined by means of light optical microscopy and density measurements. The austenitic and ferritic phase formation of the mixed alloys was significantly influenced by the chemical composition adjusted by powder mixing and the laser energy input during PBF-LB/M. The austenite content increases, on the one hand, with an increasing proportion of X2CrNiMo17-12-2 in the powder mixtures and on the other hand with increasing laser energy input. The latter phenomenon could be attributed to a slower solidification and a higher melt pool homogeneity with increasing energy input influencing the phase formation during solidification and cooling. The desired duplex microstructures could be achieved by mixing the X2CrNiMo17-12-2 powder and the X2CrNiMoN25-7-4 powder at a specific mixing ratio and building with the optimal PBF-LB/M parameters.

In recent years, magnetocaloric materials have been extensively studied as materials for use in alternative cooling systems. Shaping the magnetocaloric material to thin-walled heat exchanger structures is an important step to achieve efficient magnetocaloric cooling systems. In the present work, experimental investigations were carried out on the heat treatment of LaFe_11.4Si_1.2Co_0.4 alloy processed by Laser Beam Melting (LBM) technology. Due to the rapid solidification after melting, LBM results in a refined micro structure, which requires much shorter heat treatment to achieve a high percentage of magnetocaloric 1:13 phase compared to conventional cast material. The influence of the heat treatment parameters (temperature, time, and cooling rate) on the resulting microstructure has been extensively studied. In addition to the conventional heat treatment process, induction technology was investigated and the results were very promising in terms of achieving good magnetocaloric properties after short-time annealing. After only 15 min holding time at 1373 K, the magnetic entropy change (∆S) of -7.9 J/kg/K (0–2 T) was achieved.