Despite Fused Deposition Modeling (FDM) being an economical 3D printing method known for its material versatility and ease of use, the mechanical performance of FDM-produced components is significantly influenced by process parameter settings. This study investigated the effects of the layer thickness, raster angle, build orientation, and extrusion temperature on the ultimate tensile strength (UTS) and elastic modulus of Polylactic Acid (PLA) specimens using Taguchi methods, with significance analyzed through analysis of variance (ANOVA). The results indicated that the build orientation is the primary factor affecting both the UTS and elastic modulus, with a flat orientation yielding the best performance. ANOVA showed that the build orientation, raster angle, and extrusion temperature significantly influence the UTS, with the build orientation contributing 98.16%. For the elastic modulus, the build orientation and raster angle were significant, contributing 94.83% and 1.76%, respectively. The optimal parameters were a 0.16 mm layer thickness, flat build orientation, 30°/−60° raster angle, and 200 °C extrusion temperature, resulting in predicted UTS and elastic modulus values with error percentages of 4.33% and 2.74%, respectively, compared to experimental values. The regression model demonstrated high predictive accuracy, with R-squared values of 99.71% for the UTS and 99.52% for the elastic modulus.

Due to the high interest in the use of glass/epoxy laminates in aerospace applications, aviation, and as cryogenic tanks, it is crucial to understand the behavior of composites under challenging environmental conditions. Polymer composites are exposed to low temperatures, including cryogenic temperatures, which can lead to the initiation of microdamage. This paper investigates damage initiation/accumulation and its influence on the properties of cross-ply woven glass fiber epoxy composites at low temperatures compared to room temperature conditions. To evaluate the influence of a low-temperature environment on the mechanical performance of glass fiber reinforced epoxy composite (GFRP) laminates, three types of test campaigns were carried out: quasi-static tensile tests and stepwise increasing loading/unloading cyclic tensile tests at room temperature and in a low-temperature environment (−50 °C). We demonstrated that the initial stiffness of the laminates increased at low temperatures. On the other hand, there were no observed changes in the type or mechanism of developed damage in the two test conditions. However, the reduction in stiffness due to the accumulated damage was more significant for the laminates tested at low temperatures (~17% vs. ~11%). Exceptions were noted in a few formulations where the extent of damage at low temperatures was insignificant (<1%) compared to that at room temperature. Since some of the studied laminates exhibited a relatively minor decrease in stiffness (~2–3%), we can also conclude that the formulation of matrix material plays an important role in delaying the initiation and formation of damage.

It is commonly acknowledged that polymer composites in service are often subjected to not only intricate mechanical loads but also harsh environmental conditions. The mechanical and thermal properties of five particular composites are explored here. The composites are composed of laminates of glass cloth type “E” sheet infilled with a duroplastic matrix. This is a thermoset polymer—epoxy resin with different molecular weights. The composites were fabricated by IZOERG company, which is based in Poland. The final articles were 1.5 mm thick by 60 cm long and 30 cm wide, with the glass layers arranged parallel to the thickness. Young’s modulus and tensile strength were measured at room temperature. Using the thermal analysis of dynamic mechanical properties (DMTA), the values of the storage modulus and the loss modulus were determined, and the damping factor was used to determine the glass transition temperature (Tg). It was revealed that the nature of changes in the storage modulus, loss modulus, and damping factor of composite materials depends on the type of epoxy resin used. Thermal expansion is a crucial parameter when choosing a material for application in cryogenic conditions. Thanks to the TMA method, thermal expansion coefficients for composite materials were determined. The results show that the highest value of the coefficient of thermal expansion leads the laminate EP_4_2 based on brominated epoxy resin cured with novolac P. Duroplastic composites were characterized at cryogenic temperatures, and the results are interesting for developing cryogenic applications, including electric motors, generators, magnets, and other devices.

The article presents the thermal analysis of new, fully biodegradable thermoplastic composites filled with natural additives. The samples were made of thermoplastic material with the trade name BIOPLAST® GS 1289, and the natural filler was powder from walnut shells and chicken egg shells in various mass proportions. Differential scanning calorimetry (DSC) analysis was used to assess the quality of the new materials obtained. Moreover, it allowed to determine and select technological parameters of processing and explain the occurrence of undesirable phenomena related to the processing of these materials. The thermal properties of the obtained samples were determined using a Mettler-Toledo DSC 3 scanning calorimeter by the ISO 11357 standard. The analysis was carried out using the following method: conditioning the sample for 10 min at − 20 °C and heating from − 20 to 180 °C at a 10 K min⁻¹ speed. Each sample was subjected to three measurements according to the given method, the first and second cycle in a row, and the third cycle was performed after 24 h. The mass melt flow rate (MFR) was also determined. The critical share of filler in the matrix (BIOPLAST® GS 1289) and the influence of natural fillers on signals on the curve were determined, and it was related to the processing properties of the developed materials.

The aim of this work was to study the effect of different methods of multi-walled carbon nanotubes (MWCNTs) dispersion, and their influence on the microstructure and properties of aluminium alloy matrix composites produced using the powder metallurgy techniques, such as powder milling/mixing and hot extrusion. The main problem in the manufacturing of nanocomposites is the homogeneous distribution of MWCNTs in the metal matrix. To achieve their proper distribution a high-energy and low-energy mechanical milling, using a planetary ball mill, and mixing, using a turbulent mixer, were applied. Studies have shown that composite materials prepared using milling and extrusion have a much better dispersion of the reinforcing phase, which leads to better mechanical properties of the obtained rods. The low-energy mechanical mixing and mixing using the turbulent mixer neither change the powder morphology nor lead to adequate dispersion of the carbon nanotubes, which directly affects the resulting properties.