Additive manufacturing (AM) technology has gained significant popularity, among which Fused Deposition Modeling (FDM) has emerged as the predominant technique for 3D printing. FDM offers the unique ability to achieve the desired and tailored engineering properties required for specific applications. This experimental study investigates the influence of varying FDM process parameters on the mechanical properties and highlights the optimal set of parameters for better tensile strength for a bi-layered composite of PLA-ABS (polylactic acid and acrylonitrile butadiene styrene). Also, it investigates the most-to-least influential printing parameters. Four process parameters were played out i.e., Infill density (50%, 75%, and 100%), number of layers (20,25 and 30), printing speed (20 mm sec⁻¹, 40 mm sec⁻¹, and 60 mm sec⁻¹), and bed temperature (90 °C, 95 °C, and 100 °C), while keeping other parameters constant. Taguchi optimization technique was used for optimization and experiments were designed according to Taguchi orthogonal array L9 (3 4). After printing, the samples were evaluated for tensile properties and the results were analyzed. It is found that the infill density is the most influential parameter while bed temperature is the least influential. Infill density of 75%, 30 layers per part, a printing speed of 20 mm sec⁻¹, and a bed temperature of 100 °C are the optimal set of parameters for better tensile strength. Alongside, percent elongation, printing time, and strength-to-weight ratio were also analyzed and correlated.

Friction stir welding (FSW) is one of the primary fabrication techniques for joining different components, and it has become popular, especially in aluminum alloy structures for marine applications. The welded joint with the friction stir process greatly depends on the process parameters, i.e., feed rate, rotational speed, and pin profile of the tool. In the current study, plates of aluminum 5451 alloy were joined by the FSW technique, and the Taguchi method was used to find the process parameters at an optimal level. The maximum value of tensile strength, i.e., 160.6907 MPa, was achieved using optimum welding conditions of a tool rotation speed of 1400, a feed rate of 18 mm/min, and the tool pin with threads. The maximum value of hardness, i.e., 81.056 HV, was achieved using optimum conditions of 1200 tool rotational speed and a feed rate of 18 mm/min with a tool pin profile having threads. In addition, the contribution in terms of the percentage of each input parameter was found by the analysis of variance (ANOVA). The ANOVA results revealed that the pin profile of the tool has the maximum contribution of 67.77% and 62.42% in achieving the optimum value of tensile strength and hardness, respectively. The study also investigated the joint efficiency of the friction stir welded joint, hardness at the weld zone, and metallography on FSW samples at the optimized level. The effectiveness and reliability of FSW joints for shipping industry applications can be observed by joint efficiency. That was investigated at optimum conditions, and it comes out to be 80.5%.

To develop medical-grade stainless-steel 316L implants that are biocompatible, non-toxic and antibacterial, such implants need to be coated with biomaterials to meet the current demanding properties of biomedical materials. Hydroxyapatite (HA) is commonly used as a bone implant coating due to its excellent biocompatible properties. Zinc oxide (ZnO) nanoparticles are added to HA to increase its antibacterial and cohesion properties. The specimens were made of a stainless-steel grade 316 substrate coated with HA-ZnO using the electrophoretic deposition technique (EPD), and were subsequently characterized using scanning electron microscopy (SEM), energy dispersive X-ray (EDX), stylus profilometry, electrochemical corrosion testing and Fourier transform infrared (FTIR) spectroscopy. Additionally, cross-hatch tests, cell viability assays, antibacterial assessment and in vitro activity tests in simulated body fluid (SBF) were performed. The results showed that the HA-ZnO coating was uniform and resistant to corrosion in an acceptable range. FTIR confirmed the presence of HA-ZnO compositions, and the in vitro response and adhesion were in accordance with standard requirements for biomedical materials. Cell viability confirmed the viability of cells in an acceptable range (>70%). In addition, the antibacterial activity of ZnO was confirmed on Staphylococcus aureus. Thus, the HA-ZnO samples are recommended for biomedical applications.

Polytetrafluoroethylene (PTFE) was coated on 316L stainless steel (SS) substrate through a spin coating technique to enhance its corrosion resistance properties in hydrochloric acid (HCl) and nitric acid (HNO₃) medium. Scanning electron microscopy (SEM) revealed the morphology of the coated and uncoated substrates and showed a uniform and crack-free PTFE coating on 316L SS substrate, while a damaged surface with thick corrosive layers was observed after the electrochemical test on the uncoated sample. However, an increased concentration of HCl and HNO₃ slightly affected the surface morphology by covering the corrosive pits. An atomic force microscope (AFM) showed that the average surface roughness on 316L SS and PTFE coating was 26.3 nm and 24.1 nm, respectively. Energy dispersive X-ray spectroscopy (EDS) was used for the compositional analysis, which confirmed the presence of PTFE coating. The micro Vickers hardness test was used to estimate the hardness of 316L SS and PTFE-coated substrate, while the scratch test was used to study the adhesion properties of PTFE coating on 316L SS. The anticorrosion measurements of 316L SS and PTFE-coated substrates were made in various HCl and HNO₃ solutions by using the electrochemical corrosion test. A comparison of the corrosion performance of PTFE-coated substrate with that of bare 316L SS substrate in HCl medium showed a protection efficiency (PE) of 96.7%, and in the case of HNO₃ medium, the PE was 99.02%, by slightly shifting the corrosion potential of the coated sample towards the anodic direction.