The present article examines special steels used for the production of injection screws in the plastic industry, with a glass fiber content of up to 30%. Experimental materials, M390 and M398, are classified as tool steels, which are produced by powder metallurgy-HIP methods (hot isostatic pressing). The main goal of the presented paper is to propose the optimal tempered temperature of M398 steel and also to compare the tribological properties of both materials and to determine the degree of their wear depending on their final heat treatment. Partial results refer to the analysis of hardness, roughness, the overall wear mechanism, the change in the volume of retained austenite due to the tempering temperature, and the EDS analysis of the worn surfaces in individual contact pairs. A ceramic ball Al₂O₃ in the α phase was used as the contact material, which had a diameter of 6.35 mm. The ceramic ball performed a rotational movement on the experimental material surface at an elevated temperature of 200 °C using the dry ball-on-disk method. It was experimentally shown that the new M398 material can fully replace the M390 material because it exhibits significantly better tribological properties. The M398 material showed more than a 400% reduction in wear compared to the M390 material. The ideal heat treatment consisted of cryogenic quenching to −78 °C and a tempering temperature of 400 °C. At tempering temperatures of 200 and 400 °C, adhesive wear occurred, which was combined with abrasive wear at a tempered temperature of 600 °C. The averaged coefficient of friction (COF) results show that the M398 material presents less resistance in the friction process and its values are approximately 0.25, while the M390 material showed a COF value of 0.3 after the cryogenic hardening process. The friction surface roughness of the M398 materials also showed lower values compared to the M390 material by approximately 35%. Both of these results are related to the content of M₇C₃ and MC carbide particles based on Cr and V in the bulk of the material, which are in favor of the M398 material.

The aim of this work is to perform a detailed dilatometric analysis of the decomposition of austenite during the cooling process using experimentally derived continuous cooling transformation (CCT) diagrams for two specific tool steels, X153CrMoV12 Bohdan Bolzano, Bratislava, Slovakia and 100MnCrW4. The dilatometric curves were compared with metallographic evaluations using scanning electron microscopy (SEM). In addition, hardness measurements were performed to obtain additional information about the mechanical properties of the materials. All experimental work was performed using a DIL 805A. The accuracy of the resulting CCT diagrams was verified by comparing them with those calculated with the JMatPro software v12.4. The cooling rates ranged from 20 °C/s to 0.01 °C/s, depending on the specific type of steel tested. The novelty of this research is the combination of experimental and simulation methods to analyze the influence of alloying elements on the kinetics of phase transformations in tool steels. It was found that one of the most significant factors affecting the CCT diagrams is the weight percentage of alloying elements in the steels. These results clearly show that increasing the weight percentage of the content of alloying elements has a significant impact on the accuracy of the simulation results derived from the JMatPro software.

Additive manufacturing of polymer composites, also known as 3D printing, is one of the progressive technologies in material engineering. It enables the production of parts with complex geometries while optimizing material efficiency. Polylactide (PLA) is a widely used material in additive manufacturing due to its biodegradability and suitable mechanical properties. However, its brittleness and limited thermal stability require further modifications, such as modifying the filler structure or adding reinforcing materials. This paper focuses on analyzing the influence of different filler geometries and densities on the mechanical properties of PLA parts manufactured by the fused filament deposition (FFF) method. Three basic filler structures—cubic, gyroid and rectilinear—were investigated at different density levels from 20%, 40%, 60% and 80%. Experimental tests were performed according to ASTM D638 to determine the strength characteristics of the material. In addition to mechanical tests, dynamic mechanical analysis (DMA) and thermogravimetric analysis (TG) were performed to better understand the influence of the filling geometry on the thermal stability and viscoelastic behavior of the material. Experimental tests according to ASTM D638 showed that higher filling density improves mechanical properties. At 80% filling, the tensile strength reached 21.06 MPa (cubic), 20.53 MPa (gyroid) and 20.84 MPa (linear). The elastic modulus was highest with cubic filling (1414.19 MPa). The yield strength reached 15.59 MPa (cubic), 15.52 MPa (gyroid) and 14.30 MPa (linear).

Effect of nitrogen on surface morphology of layers

Influence of alloying elements on gas nitriding process of high-stressed machine parts of weapons

The influence of plasma nitriding and gas nitriding processes on the change of surface roughness and dimensional accuracy of 42CrMo4 steel was investigated in this paper. Both processes almost always led to changes in the surface texture. After plasma nitriding, clusters of nitride ions were formed on the surface of steel, while gas nitriding very often led to the new creation of a formation of a “plate-like” surface texture. In both cases of these processes, a compound layer in specific thickness was formed, although the parameters of the processes were chosen with the aim of suppressing it. After the optimizing of nitriding parameters during nitriding processes, it was found that there were no changes in the surface roughness evaluated using the Ra parameter. However, it turned out that when using a multi-parameter evaluation of roughness (the parameters Rz, Rsk and Rku were used), there were presented some changes in roughness due to nitriding processes, which affect the functional behavior of the components. Roughness changes were also detected by evaluating surface roughness profiles, where nitriding led to changes in peak heights and valley depths. Nitriding processes further led to changes in dimensions in the form of an increase of 0.032 mm on average. However, the magnitude of the change has some context on chemical composition of material. A larger increase in dimensions was found with gas nitriding. The change in the degree of IT accuracy is closely related to the change in dimension. For both processes, there was a change of one degree of IT accuracy compared to the ground part (from IT8 to IT9). On the basis of the achieved dimensional accuracy results, a coefficient of change in the degree of accuracy IT was created, which can be used to predict changes in the dimensional accuracy of ground surfaces after nitriding processes in degrees of accuracy IT3–IT10. In this study, a tool for predicting changes in degrees of accuracy of ground parts after nitriding processes is presented.