In this study, the environmentally friendly friction stir processing (FSP) method was utilized to fabricate surface composites employing technical aluminum matrix 1050-H14 and aluminum alloy 6060-T4 reinforced with silicon carbide (SiC) particles. Microstructure analysis, employing light and scanning electron microscopy, in conjunction with comprehensive evaluations of hardness, compressive strength, and tribological properties, was conducted to elucidate significant findings. The results reveal that an augmented number of FSP passes contributes to the homogenization of microstructure, leading to the alteration of SiC particle morphology and fragmentation. Consequently, this phenomenon results in improved mechanical properties, particularly noteworthy in the case of AA6060-T4 alloy matrix composites, and enhanced wear resistance. Both AA1050-SiC and AA6060-SiC composites demonstrate notable increases in compressive strength compared to their unreinforced matrices. Particularly noteworthy is the substantial enhancement in compressive strength observed in the AA6060-SiCp composite, escalating from 249 to 331 MPa (at ε = 0.1) and from 398 to 715 MPa (at ε = 0.2) with an increase in the number of FSP passes. Additionally, FSP’s ability to precisely control process parameters such as tool rotational speed and traverse speed allows for the optimization of mechanical properties and microstructural characteristics tailored to specific application requirements. This study highlights the potential of FSP in fabricating high-performance aluminum matrix composites with superior strength and wear resistance, positioning it as a viable technique for advanced engineering applications. The environmentally friendly nature of FSP, due to its solid-state operation and reduced energy consumption, further underscores its suitability for sustainable manufacturing practices.

The paper presents the results of the joining tests of the EN AW-6082 T6 alloy. The materials were joined using the EBW high-energy (electron beam welding) and friction stir welding (FSW) methods. In the case of FSW welding, the following parameters were used: the linear speed was 355 mm/min, and the rotational speed of the welding tool was 710. In the case of EBW welding, the following parameters were used: accelerating voltage U = 120 kV, beam intensity I = 18.7 mA, welding speed v = 1600 mm/min and, in the case of a smoothing weld, U = 80 kV, beam intensity I = 17 mA, and welding speed v = 700 mm/min. Comprehensive microstructural tests of all welded joints (MO, SEM and TEM) and mechanical property tests (tensile and hardness tests) were carried out. The topographies of the fractures after the tensile test were also examined. Based on the results, it was found that the strength properties of the EBW joint were reduced by 23% and the FSW joint by 38% compared to the base material. A decrease in elongation was also noted, with an FSW elongation of 7.2% and an elongation of 2.7% for EBW. In the case of the EBW joint, magnesium evaporation was found in the weld during welding, while in the FSW joint, the dissolution of the Mg2Si particles responsible for strengthening the material during heat treatment to the T6 state was observed.

For the friction stir welding (FSW) of AZ91 magnesium alloy, low tool rotational speeds and increased tool linear speeds (ratio 3.2) along with a larger diameter shoulder and pin are utilized. The research focused on the influence of welding forces and the characterization of the welds by light microscopy, scanning electron microscopy with an electron backscatter diffraction system (SEM-EBSD), hardness distribution across the joint cross-section, joint tensile strength, and SEM examination of fractured specimens after tensile tests. The micromechanical static tensile tests performed are unique and reveal the material strength distribution within the joint. A numerical model of the temperature distribution and material flow during joining is also presented. The work demonstrates that a good-quality joint can be obtained. A fine microstructure is formed at the weld face, containing larger precipitates of the intermetallic phase, while the weld nugget comprises larger grains. The numerical simulation correlates well with experimental measurements. On the advancing side, the hardness (approx. 60 HV0.1) and strength (approx. 150 MPa) of the weld are lower, which is also related to the lower plasticity of this region of the joint. The strength (approx. 300 MPa) in some micro-areas is significantly higher than that of the overall joint (204 MPa). This is primarily attributable to the macroscopic sample also containing material in the as-cast state, i.e., unwrought. The microprobe therefore includes less potential crack nucleation mechanisms, such as microsegregations and microshrinkage.

This study investigates the physical and mechanical properties of biodegradable composites based on PLA/PHBV blends modified with different content of nanocrystalline cellulose (NCC) of 5, 10, and 15 wt.%. Density measurements reveal that the density of the composite increases with increasing NCC content. Water absorption tests demonstrate a gradual increase in the composite water content with increasing incubation time, reaching stabilization after approximately 30 days. Mechanical testing was also carried out on both on conditioned samples after the process of hydrolytic degradation and accelerated thermal aging. The conditioned composites show an increase in the stiffness of the materials with increasing content of nanocrystalline cellulose. The ability to deform and the ability to absorb energy when the sample is dynamically loaded decrease. The repeated strength tests, after the process of incubation of samples in water and after the process of accelerated thermal aging, show the degradation of composite materials; however, it is noticed that the introduction of cellulose addition reduces the impact of the applied artificial environment in aging tests. The findings of this study indicate promising applications for these types of materials, characterized by high strength and biodegradability under appropriate conditions. Household items such as various containers or reusable packaging represent potential applications of these composites.

One of the new areas that requires extensive study of the structure and properties of welded joints is the heat-affected zone (HAZ). This issue is particularly important for new constructions made of aluminium alloys intended for battery housing for powering electric car engines. Modern welding methods, such as EBW and FSW, meet the requirements related to the high precision of the process and the quality of the welded joint itself. This article presents the results of an analysis of the structure and strengthening of the HAZ of chemically modified AlMgSi(Cu) alloys via EBW and FSW. Microstructural observation was performed via SEM for each welded joint to determine the morphology of the precipitates. In the HAZ, β-Mg₂Si, Q-Al,MgCu,Si and α-Al,Fe,Si (Mn,Cu) phases with larger sizes and rounded shapes were visible than they were directly in the weld made via the EBW method. The joints produced by the FSW method were characterised by a wide weld area and an irregular weld line. Analysis of the crystallographic orientation via EBSD and grain orientation spread (GOS) revealed differences in the shape of the grains and the degree of recrystallisation in the weld area between the FSW and EBW methods. The distributions of HB (FSW) hardness and HV (EBW) microhardness measurements revealed a slight decrease in hardening in the HAZ. In joints welded by both methods, the hardness of the welds for alloys with increased copper and chromium contents increased by approximately 5%.